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Method for preparing abalone shell pearl layer powder

A technology of nacre powder and abalone shell, which is applied in skin care preparations, medical preparations containing active ingredients, and pharmaceutical formulas, etc. It can solve the problems of ingredient damage and discount of medicinal value, and achieve endocrine regulation and absorption rate improvement. , the effect of promoting metabolism

Inactive Publication Date: 2011-04-06
FUZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

So now the actual situation is: Many factories only use strong alkaline substances such as NaOH to remove the outer cuticle and then crush it. The pearl layer powder obtained by these low-cost methods is easy to be destroyed, and its medicinal value will be reduced. big discount

Method used

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  • Method for preparing abalone shell pearl layer powder
  • Method for preparing abalone shell pearl layer powder

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The preparation method of abalone shell pearl layer powder of the present invention, concrete steps are as follows:

[0025] (1) Soak the abalone shell with 10% (volume ratio) hydrochloric acid solution for 10 hours, then peel off the outer layer of the abalone shell, and then soak the abalone shell with 2% (volume ratio) hydrogen peroxide for 2 hours to obtain the nacre of the abalone shell with pearly luster;

[0026] (2) Crush the abalone shell nacre and sieve it through a 200-mesh filter to obtain ground abalone shell nacre powder;

[0027] (3) Dissolve the abalone shell pearl layer grinding powder in 2% (volume ratio) acetic acid solution, and keep stirring until no more bubbles are generated, then centrifuge at 6000rpm for 30min, collect the supernatant and precipitate respectively; concentrate the supernatant Freeze-dried to obtain powder P 1 ;

[0028] (4) Soak the precipitate collected in step (3) with 40% (weight ratio) NaOH solution at 120°C for 3 days, the...

Embodiment 2

[0032] The preparation method of abalone shell pearl layer powder of the present invention, concrete steps are as follows:

[0033] (1) Soak the abalone shell with 50% (volume ratio) lactic acid for 6 hours, then peel off the outer layer of the abalone shell, and then soak the abalone shell with 5% (volume ratio) hydrogen peroxide for 1 hour to obtain the nacre of the abalone shell with pearly luster;

[0034] (2) Crush the abalone shell nacre and sieve it through a 200-mesh filter to obtain ground abalone shell nacre powder;

[0035] (3) Dissolve the abalone shell pearl layer grinding powder in 10% (volume ratio) lactic acid solution, and keep stirring until no more bubbles are generated, then centrifuge at 8000rpm for 10min, collect the supernatant and precipitate respectively; concentrate the supernatant Freeze-dried to obtain powder P 1 ;

[0036] (4) Soak the precipitate collected in step (3) with 60% (by weight) KOH solution at 80°C for 7 days, then centrifuge at 8000r...

Embodiment 3

[0040] The preparation method of abalone shell pearl layer powder of the present invention, concrete steps are as follows:

[0041] (1) Soak the abalone shell with 25% (volume ratio) acetic acid solution for 9 hours, then peel off the surface layer of the abalone shell, and then soak the abalone shell with 3% (volume ratio) hydrogen peroxide for 1.5 hours to obtain the nacre of the abalone shell with pearly luster;

[0042] (2) Crush the abalone shell nacre and sieve it through a 200-mesh filter to obtain ground abalone shell nacre powder;

[0043] (3) Dissolve the abalone shell pearl layer grinding powder in 6% (volume ratio) lactic acid solution, and keep stirring until no more bubbles are generated, then centrifuge at 6000rpm for 20min, collect the supernatant and precipitate respectively; concentrate the supernatant Freeze-dried to obtain powder P1 ;

[0044] (4) Soak the precipitate collected in step (3) with 50% (by weight) NaOH solution at 100°C for 5 days, then centri...

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PUM

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Abstract

The invention provides a method for preparing abalone shell pearl layer powder. The method comprises the following steps of: soaking abalone shells into acid solution to obtain abalone shell pearl layers, performing grinding, acid dissolution and alkali soaking, and dissolving in acid solution to obtain the abalone shell pearl layer powder. Compared with the prior process for preparing the abalone shell pearl layer powder, the method of the invention has the advantages that: the obtained abalone shell pearl layer powder keeps all components of the abalone shell pearl layers, and the soluble powder keeps most components of a biological sample. Compared with a water-soluble pearl powder production method, the method has simple preparation process, and can greatly reduce the production cost and relieve environmental pollution and energy consumption.

Description

technical field [0001] The invention relates to a preparation method of abalone shell pearl layer powder. Background technique [0002] Nacre, also known as hypostracum, is the innermost structure of the shell of molluscs (such as mussels). It is usually shiny and has strong refractive reflection. [0003] Nacre powder is ground into powder from the inner layer of mollusc shells. Nacre powder and pearl powder are homologous and contain the same ingredients as pearls, mainly calcium, sugars, various amino acids and A small amount of trace elements, the keratin contained in it has a variety of amino acid components that cannot be produced by the human body. Pearl layer powder has multiple functions such as applying the face to remove freckles, treating skin allergies, removing acne, and moisturizing the skin. [0004] The cost of nacre powder itself is very low. In order to obtain nacre, the cuticle on the outer surface of the shell and the prismatic layer in the middle mu...

Claims

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Application Information

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IPC IPC(8): A61K35/56A61K8/98A61P17/00A61Q19/08A61K35/618
Inventor 张其清王志力
Owner FUZHOU UNIV
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