Enzymatically synthesized triglyceride type fish oil soft capsules and preparation method thereof
An enzymatic synthesis, triglyceride technology, applied in the direction of capsule delivery, non-active ingredients of polymer compounds, drug combination, etc., can solve problems such as rising to 2.5 or even higher, unqualified capsule products, etc.
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Embodiment 1
[0026] a. Sol process: put 250 g / 1000 grains of distilled water into the container, use steam to heat to 80°C, add 98g / 1000 grains of glycerin and 244 g / 1000 grains of vegetable glue, then control the temperature to 70°C and vacuum to 0.05Mpa. Stir and defoam for 15 minutes; control the temperature at 75°C, stir and dissolve for 15 minutes; then control the temperature at 65°C, vacuum degree 0.09Mpa, defoam and concentrate for 20 minutes; The water content of the liquid is 40%, and the glue is kept at 45°C.
[0027] b. Ingredients process: Take 510 g / 1000 capsules of enzymatically synthesized fish oil, including 65% triglyceride, 28% diglyceride, 1.5% monoglyceride, and 5.5% ethyl ester; filter through 120 mesh, add natural vitamin E oil 2g / 1000 granules, stir for 40 minutes to make it evenly mixed and set aside.
[0028] c, pill pressing qualitative: control pill chamber temperature 20%, relative humidity 45%, loading is controlled at 500mg, and product specification is 500m...
Embodiment 2
[0034] a. Sol process: put 400 g / 1000 grains of distilled water into a container, use steam to heat to 80°C, add 150g / 1000 grains of glycerin and 244g / 1000 grains of animal glue, then control the temperature at 80°C, vacuum degree 0.05Mpa, and stir Degassing for 25 minutes; control the temperature at 80°C, stir and dissolve for 20 minutes; then control the temperature at 75°C, vacuum degree 0.09Mpa, defoam and concentrate for 25 minutes; finally, at 70°C, filter the glue through a 120-mesh filter bag to obtain the glue The water content is 40%, and the glue solution is kept at 45°C.
[0035] b. Ingredients process: Take 700 g / 1000 grains of enzymatically synthesized fish oil, which contains 75% triglyceride, 19% diglyceride, 1.5% monoglyceride, and 6% ethyl ester; filter through 120 mesh, add natural vitamin E oil 4g / 1000 granules, stir for 50 minutes to make it evenly mixed and set aside.
[0036] c, pill pressing qualitative: control pill chamber temperature 20%, relative h...
Embodiment 3
[0042] a. Sol process: take 580 g / 1000 capsules of distilled water and put it into a container, heat it to 80°C with steam, add 200g / 1000 capsules of glycerin and 244 g / 1000 capsules of collagen glue, then control the temperature at 80°C and vacuum degree of 0.05Mpa , stirring and defoaming for 30 minutes; controlling the temperature at 85°C, stirring and dissolving for 30 minutes; then controlling the temperature at 80°C and vacuum degree of 0.09Mpa, defoaming and concentrating for 30 minutes; The moisture content of the glue is 40%, and the glue is kept warm at 45°C.
[0043] b. Ingredients process: Take 510 g / 1000 grains of enzymatically synthesized fish oil, which contains 80% triglyceride, 15% diglyceride, 2.5% monoglyceride, and 2.5% ethyl ester; filter through 120 mesh, add natural vitamin E oil 5g / 1000 granules, stir for 70 minutes to make it evenly mixed and set aside.
[0044] c, pill pressing qualitative: control pill chamber temperature 20%, relative humidity 45%,...
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