Construction of abrin A chain mutant and application as candidate vaccine antigen
A technology of vaccines and recombinant vectors, applied in antiviral agents, recombinant DNA technology, medical preparations containing active ingredients, etc.
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Embodiment 1
[0031] Embodiment 1, the acquisition of mutant mATA
[0032] 1. Obtaining of mutant mATA
[0033] According to the existing A-chain gene (rATA) sequence of abrin toxin (rATA nucleotide sequence is sequence 5, rATA amino acid sequence is sequence 6), using Quickchange Lighting Site-Directed Mutagenesis Kit (Stratagene Company, Catalog#210518) to carry out The mutant mATA-E164AR167L (plasmid) was obtained by site-directed mutagenesis. After sequencing, the gene contained in mATA-E164AR167L was named mATA. The 1-753rd nucleotide sequence of the terminal; the amino acid sequence of mATA encoded protein mATA is the sequence shown in Sequence 2 in the sequence list. Using Lasergene software to predict the antigenicity of the constructed mutants did not change significantly.
[0034] The mutation results were verified by sequencing, as follows:
[0035] The base A at the 491st position of sequence 5 is mutated to the base C at the 491st position of the sequence 1, and the base G a...
Embodiment 2
[0050] Embodiment 2, the biological activity detection of mutant mATA
[0051] 1. Quantification of Mutant Proteins
[0052] The purified mATA obtained in Example 1 was quantified using the BCA method protein quantification kit (purchased from Beijing Biotech Biotechnology Co., Ltd., Lot #20120613). The experiment was repeated three times, and the results were averaged.
[0053] Specific steps:
[0054] Kit composition: protein standard (5mg / mlBSA), Solution A, Solution B.
[0055] (1) When using, shake and mix Solution A. According to the number of samples, prepare an appropriate amount of BCA working solution with 50 volumes of Solution A plus 1 volume of Solution B (50:1), and mix well.
[0056] (2) Completely dissolve the protein standard (5mg / mlBSA), dilute it to 1.5mg / ml, 1.0mg / ml, 0.8mg / ml, 0.4mg / ml, 0.2mg / ml with PBS as the standard.
[0057] (3) Add the standard substance and the sample to be tested at each concentration mentioned above to the 96-well plate respect...
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