Near infrared spectrum based detection method for rapid discrimination of oil-tea camellia seed oil real property

A near-infrared spectroscopy and near-infrared spectrometer technology is applied in the field of detection of the true properties of pure camellia oleifera seed oil, which can solve the problems of complex tea oil detection methods, long detection time, cumbersome operation, etc., and achieve good research and application prospects and detection process. The effect of short time and easy control

Active Publication Date: 2011-11-23
HUNAN AGRI PRODS PROCESSING INST
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Problems solved by technology

However, chemical qualitative analysis methods sometimes cannot accurately judge the purity of camellia oil, and it may be necessary to use chromatographic analysis methods to determine the fatty acid composition of oils and fats at the same time.
These shortcomings limit the determination of fatty acids in a large number of samples. It is necessary to find a simple, fast and high-precision qualitative method to identify the true properties of Camellia oleifera seed oil to ensure the quality of camellia oil
[0004] Near-infrared spectroscopy is a new technology that has emerged in the field of detection applications in recent years. It has appli

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  • Near infrared spectrum based detection method for rapid discrimination of oil-tea camellia seed oil real property
  • Near infrared spectrum based detection method for rapid discrimination of oil-tea camellia seed oil real property
  • Near infrared spectrum based detection method for rapid discrimination of oil-tea camellia seed oil real property

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Embodiment

[0029] A detection method for quickly identifying the true attributes of camellia oleifera seed oil based on near-infrared spectroscopy of the present invention, specifically comprising the following steps:

[0030] 1. Establishment of Camellia oleifera seed oil identification analysis model

[0031]1.1 Sample selection and determination of its true attributes: randomly select 163 different camellia oleifera seed oil samples, and use gas chromatography to measure the fatty acid composition and relative percentage content in each camellia oleifera seed oil sample. The gas chromatographic method used in this example According to "GB / T 17376-2008 Fatty Acid Methyl Esters Preparation of Animal and Vegetable Fats and Fats", specifically refers to: Weigh 60 mg of each sample oil sample into a 10 mL stoppered test tube, pipette 4 mL of isooctane dissolved oil Then add 200 μL potassium hydroxide methanol solution (2 mol / L) with a micropipette, cover with a glass stopper and shake vigo...

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Abstract

The invention discloses a near infrared spectrum based detection method for rapid discrimination of oil-tea camellia seed oil real property. The method comprises the following steps: first, a near infrared spectrometer is used to acquire spectrum data of an oil-tea camellia seed oil sample to be detected, and a near infrared spectrum scan wave number, a near infrared spectrum scan frequency and a resolution are controlled during acquisition; then data with spectral band within 5750-6000cm<-1> are selected from an acquired standard spectrum and treated with a smoothing, a first derivative processing and a self-normalization; at last the data is input into an oil-tea camellia seed oil discrimination and analysis model, and a mahalanobis distance discrimination method is employed to determine whether a sample point falls in a delimited real sample area in the oil-tea camellia seed oil discrimination and analysis model, so as to determine true or false of the sample to be detected. The detection method of the invention has advantages of simple operation, rapid detection, safety, environmental protection, and high precision.

Description

technical field [0001] The invention relates to a method for detecting camellia oil, in particular to a method for detecting the real property of pure camellia oleifera seed oil. Background technique [0002] Camellia oleifera is a plant of the genus Camellia in the family Theaceae, and it is a unique oil tree species in my country. The planting area of ​​camellia oleifera forest in my country is about 4 million ha 2 , mainly distributed in the southern provinces of Hunan, Jiangxi, Guangxi, Zhejiang, Fujian, Anhui and Guizhou, accounting for more than 80% of the planting area of ​​woody oil plants in the country, with an annual output of more than 600,000 tons of Camellia oleifera seeds. [0003] At present, the varieties of tea oil on the market include 100% wild camellia oil, 100% tea seed oil, tea seed (rapeseed) blended oil, etc. In order to promote the improvement of the quality of tea oil and prevent adulteration, for 100% pure camellia oil, "GB 11765-2003 Camellia Se...

Claims

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Application Information

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IPC IPC(8): G01N21/25
Inventor 张菊华朱向荣尚雪波苏东林张群帅鸣
Owner HUNAN AGRI PRODS PROCESSING INST
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