Reduced pressure distillation method and device
A distillation method and vacuum distillation tower technology, applied in the field of petroleum refining, can solve the problems of thermal stress safety design and installation difficulty, unfavorable vacuum distillation tower operation, etc., to improve the gas-liquid separation of feed and save equipment investment , Reduce the effect of condensation and vacuum load
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Embodiment 1
[0035] The method of the invention is used in the design of a new crude oil atmospheric and vacuum device.
[0036] The processing capacity of the decompression unit is 1.2 million tons per year, and the decompression process includes a decompression furnace, a flash tower, and a decompression tower. The decompression tower is a structured packing tower, which adopts wet process operation. The steam blowing volume at the bottom of the tower is 1% of the tower feed, the operating pressure at the top of the tower is 1.315kPa, and the pressure drop of the whole tower is 600Pa~750Pa.
[0037] The normal bottom oil is fed into the vacuum distillation unit at a rate of 150 tons per hour, heated to 390°C to 400°C by a vacuum furnace, and then enters the vacuum flash tower. The oil transfer line is canceled, the flash tower is directly connected with the vacuum tower, and the pressure of the flash tower is 10kPa. After adiabatic flash evaporation, the flash top gas accounts for 45.67...
Embodiment 2
[0043] The method of the present invention is used for the expansion and transformation of a certain crude oil atmospheric and vacuum device. The normal pressure part is the same as the conventional atmospheric and vacuum device, and the decompression part mainly includes a decompression furnace, a flash tower and a decompression tower.
[0044] The decompression tower is a structured packing tower, the operating pressure at the top of the tower is 1.315kPa, and the pressure drop of the whole tower is 600Pa~750Pa.
[0045] The normal bottom oil enters the vacuum distillation unit, is heated to 390°C to 400°C by a vacuum furnace, and then enters the vacuum flash tower. Cancel the oil transfer line, the flash tower is directly connected with the vacuum tower, the pressure of the flash tower is 10kPa, the flash top gas accounts for 45.67% of the feed after the adiabatic flash, the flash bottom oil enters the vacuum tower 15, and the side line of the vacuum tower The products 10, ...
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