Preparation process for schisandrol extract

A preparation process and technology of pentanol is applied in the field of preparation technology of pentanol extract, which can solve the problems of affecting curative effect and inability to extract effective components, and achieve the effects of significant curative effect, improved purity and good quality.

Inactive Publication Date: 2012-10-10
安徽海神寿春药业有限公司
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  • Abstract
  • Description
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Problems solved by technology

However, the existing preparation process cannot completely extract the active ingredients, thus affecting the curative effect

Method used

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Experimental program
Comparison scheme
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Embodiment Construction

[0025] The present invention will be further described below in conjunction with embodiment.

[0026] The preparation process of Wurenol extract comprises the following steps:

[0027] ①, pre-processing

[0028] Schisandra is depulped, dried, and crushed into coarse powder.

[0029] ②, extraction

[0030] Schisandra seed coarse powder, add 85% ethanol (volume percentage content, the same below) of 5 times the weight ratio, reflux extraction 3 times, 2 hours each time.

[0031] ③ Concentration

[0032] Ethanol is recovered from the extract in a single-effect concentrator to a relative density of 1.15-1.20.

[0033] ④, refluxing extraction

[0034] Add ethanol to the concentrate to make the alcohol content reach 85%, and reflux for 1 hour.

[0035] ⑤, alcohol precipitation

[0036] The refluxed ethanol extract was pumped into an alcohol precipitation tank, stirred for 15 minutes, and left to stand for 48 hours.

[0037] ⑥, re-concentration

[0038] Take the supernatant ...

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Abstract

The invention discloses a preparation process for a traditional Chinese medicine extract and particularly relates to a preparation process for a schisandrol extract. The preparation process for the schisandrol extract comprises the following steps of pretreatment, extraction, concentration, reflux extraction, ethanol precipitation, reconcentration and drying. The schisandrol extract prepared by the preparation process has a medicinal function of lowering serum glutamic pyruvic transaminase and is used for treating chronic hepatitis. Verified by experiments, schisandrin b and total lignans only can be fully extracted in 85 percent of alcohol. When the extraction is performed by adopting the alcohol with other concentrations, active constituents cannot be completely extracted, and then, the curative effect is influenced. Meanwhile, by adopting the ethanol precipitation process in the preparation process disclosed by the invention, impurities, such as grease, can be removed, so that the purity is greatly increased, the quality is higher, and the curative effect is comparatively obvious.

Description

technical field [0001] The invention discloses a preparation process of a traditional Chinese medicine extract, in particular to a preparation process of Wurenol extract. Background technique [0002] In the prior art, the preparation of Wurenol extract is mainly realized by extraction. However, the existing preparation process cannot completely extract the active ingredients, thereby affecting the curative effect. Contents of the invention [0003] In view of the above-mentioned situation existing in the background technology, the object of the present invention is to provide a kind of Wuren alcohol extract preparation process. [0004] The technical scheme that the present invention adopts is as follows: [0005] The preparation process of Wurenol extract is characterized in that it comprises the steps: [0006] ①, pre-processing [0007] Schisandra chinensis is depulped, dried, and crushed into coarse powder; [0008] ②, extraction [0009] Schisandra seed coarse ...

Claims

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Application Information

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IPC IPC(8): A61K36/57A61P1/16A61K131/00
Inventor 黄河陈家齐于峰李勇
Owner 安徽海神寿春药业有限公司
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