Radiating paint, and preparation method and application thereof
A technology of heat-dissipating paint and organic solvent, applied in coating and other directions, can solve the problems of poor heat-dissipation effect, large volume, occupation and so on
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[0035] Preparation of Preliminary Example 1 Nano-Silicon-Al-Carbon-Oxygen Alloy Powder
[0036] Weigh each raw material according to the stated weight: nano-aluminum powder (average particle size 50-200nm) 300 kg, nano-silicon powder (average particle size 50-200nm) 100 kg, nano-carbon powder (average particle size 50-200nm) 80 kg , 1000 kg of 100% ethanol, 1 kg of concentrated hydrochloric acid, 10 kg of silane coupling agent KH-570 (purchased from Nanjing Qianqian Chemical Co., Ltd., trade name: silane coupling agent KH-570);
[0037] Put concentrated hydrochloric acid into 100% ethanol and stir for 10 minutes to dissolve, then fill the reactor with nitrogen to catch oxygen, nitrogen bubbles under the liquid surface, after 2 hours, add nano-aluminum powder, nano-silicon powder, nano-carbon powder, stir for 1 hour, add KH-570, and stir for 16 hours; then centrifuge and dry to obtain a good mixed powder with surface treatment (the X-ray diffraction pattern is shown in figure ...
Embodiment 2
[0038] Preparation of Preliminary Example 2 Nano-Silicon-Al-Carbon-Oxygen Powder
[0039] Weigh each raw material according to the stated weight: 200 kg of nano-aluminum powder (average particle size 50-200nm), 50 kg of nano-silicon powder (average particle size 50-200nm), 100 kg of nano-carbon powder (average particle size 50-200nm) , 500 kg of isopropanol, 1 kg of concentrated sulfuric acid, 2 kg of silane coupling agent KH-570 (purchased from Nanjing Xiangqian Chemical Co., Ltd., trade name: silane coupling agent KH-570);
[0040] Put concentrated sulfuric acid into isopropanol and stir for 10 minutes to dissolve, then fill the reaction vessel with nitrogen to catch oxygen, nitrogen bubbles under the liquid surface, after 2 hours, add nano-aluminum powder, nano-silicon powder, nano-carbon powder, stir for 1 hour, add KH-570, stir for 24 hours; then centrifuge, dry the precipitated powder at 80-150 °C in the absence of oxygen to obtain a mixed powder with surface treatment, ...
Embodiment 3
[0041] Preparation of Preliminary Example 3 Nano-Silicon-Al-Carbon-Oxygen Alloy Powder
[0042] Weigh each raw material according to the stated weight: nano-aluminum powder (average particle size 50-200nm) 1000 kg, nano-silicon powder (average particle size 50-200nm) 500 kg, nano-carbon powder (average particle size 50-200nm) 300 kg , 2000 kg of xylene, 20 kg of ammonia water, 15 kg of silane coupling agent KH-570 (purchased from Nanjing Qianqian Chemical Co., Ltd., trade name: silane coupling agent KH-570);
[0043]Put ammonia into xylene and stir for 20 minutes to dissolve, then fill the reactor with nitrogen to catch oxygen, nitrogen bubbles under the liquid surface, after 2 hours, add nano-aluminum powder, nano-silicon powder, nano-carbon powder, stir for 2 hours, Add KH-570 and stir for 36 hours; then centrifuge, and dry the precipitated powder at 100°C in the absence of oxygen to obtain a mixed powder with surface treatment, and burn the powder at 1200°C in a tunnel furn...
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