Mechanically plated pellets and method of manufacture
A technology of mechanical plating and pellets, applied in chemical instruments and methods, pressure inorganic powder plating, transportation and packaging, etc., can solve problems such as high cost, difficult manufacturing, high risk of mercury exposure, etc.
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Embodiment 1a
[0157] Example 1a: Improved Zn-Hg pellets
[0158] The premix was prepared by adding 1000 g of vacuum dried Zn powder (5-8 μm particle size) and 1000 g of high purity mercury into an argon filled vessel which was 1 / 4 full when both were added. The mixture was shaken for 5 minutes.
[0159]The second container was filled 1 / 3 full with 175g of 2mm glass beads. The premix was then added to the glass bulb, shaking for 30-40 seconds between premix additions. The pellets are substantially round and have a uniform composition.
Embodiment 1b
[0160] Example 1b: Zn-Hg combination by mechanical plating and by melt-based techniques thing
[0161] The compositions of 10 batches of melt-based Zn-Hg and 10 batches of mechanically plated Zn-Hg were measured by inductively coupled plasma (ICP) mass spectrometry. Within experimental limits, the average Hg composition of the mechanically plated material is closer to the targeted 50% value than the melt-based Zn-Hg.
Embodiment 2
[0163] This example compares the yield of a melt-based method with that of a mechanical plating method. The yield was measured from 11 batches of melt-based Zn-Hg, and the average yield was determined to be 70%.
[0164] The yield was measured from 9 batches of mechanically plated Zn-Hg and the average yield was determined to be 99%. Therefore, mechanical plating yields much higher yields.
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