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Mechanically plated pellets and method of manufacture

A technology of mechanical plating and pellets, applied in chemical instruments and methods, pressure inorganic powder plating, transportation and packaging, etc., can solve problems such as high cost, difficult manufacturing, high risk of mercury exposure, etc.

Inactive Publication Date: 2013-01-23
ADVANCED LIGHTING TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Melt-based methods are generally associated with relatively high cost, relative difficulty in fabrication, and relatively high risk of mercury exposure

Method used

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  • Mechanically plated pellets and method of manufacture
  • Mechanically plated pellets and method of manufacture
  • Mechanically plated pellets and method of manufacture

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1a

[0157] Example 1a: Improved Zn-Hg pellets

[0158] The premix was prepared by adding 1000 g of vacuum dried Zn powder (5-8 μm particle size) and 1000 g of high purity mercury into an argon filled vessel which was 1 / 4 full when both were added. The mixture was shaken for 5 minutes.

[0159]The second container was filled 1 / 3 full with 175g of 2mm glass beads. The premix was then added to the glass bulb, shaking for 30-40 seconds between premix additions. The pellets are substantially round and have a uniform composition.

Embodiment 1b

[0160] Example 1b: Zn-Hg combination by mechanical plating and by melt-based techniques thing

[0161] The compositions of 10 batches of melt-based Zn-Hg and 10 batches of mechanically plated Zn-Hg were measured by inductively coupled plasma (ICP) mass spectrometry. Within experimental limits, the average Hg composition of the mechanically plated material is closer to the targeted 50% value than the melt-based Zn-Hg.

Embodiment 2

[0163] This example compares the yield of a melt-based method with that of a mechanical plating method. The yield was measured from 11 batches of melt-based Zn-Hg, and the average yield was determined to be 70%.

[0164] The yield was measured from 9 batches of mechanically plated Zn-Hg and the average yield was determined to be 99%. Therefore, mechanical plating yields much higher yields.

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Abstract

Mechanical plating provides a new technique of manufacturing of certain materials containing multiple elements, including amalgams, and novel pellets containing multiple materials. Some embodiments provide new and versatile materials for dosing mercury, metals or other inorganic compounds into lamps. Some embodiments include materials comprising layers of metals or compounds built up on a substrate. One embodiment is a layer of zinc amalgam applied to a glass sphere. Also disclosed is an improved method of manufacture for such particles that will speed production, increase yields, lower costs and reduce exposure to mercury in the workplace.

Description

[0001] Cross References to Related Applications [0002] This application claims priority under 35 U.S.C. §119(e) to U.S. Provisional Patent Application Serial No. 61 / 322,691, filed April 9, 2010, which application is hereby incorporated by reference in its entirety. Background technique [0003] In various industries and technologies, there is a need to provide precise and small quantities of various materials. In the lighting industry, for example, a small amount of mercury has to be fed into the discharge vessel of a fluorescent lamp. Mercury can be introduced into the discharge lamp in the form of solid amalgam particles. Particles used to provide small amounts of material may be referred to as pellets. A known technique for making and using amalgam pellets to dose mercury into discharge lamps is described in Anderson, U.S. Patent 4,419,303, "Method for producing large diameter high purity sodium amalgam particles The melt-based (falling tower) technique in "Aligning Pa...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C24/02B22F1/18
CPCH01J61/28H01J61/00C22C1/0483H01J61/20H01J9/395C22C1/0491H01J7/20C09K11/00C23C24/045B22F1/025Y10T428/2998Y10T428/2991B22F1/18C22C1/047
Inventor D·J·高登S·C·汉森T·I·艾米尔森T·R·布拉姆勒夫
Owner ADVANCED LIGHTING TECH
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