Preparation method of composite material of epoxy resin and closed-cell foamed aluminum

A technology of closed-cell aluminum foam and epoxy resin, which is applied in the field of composite materials, can solve the problems of waste of resources and energy, high production costs, and low yield strength, and achieve reduced environmental pollution, good mechanical properties, and good energy absorption effects Effect

Inactive Publication Date: 2013-05-22
TANGSHAN HAODONG PRECISION MACHINERY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention is to provide a preparation method of epoxy resin and closed-cell foamed aluminum composite material, which is a preparation method of dispersed embedded epoxy resin and closed-cell foamed aluminum composite mat

Method used

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  • Preparation method of composite material of epoxy resin and closed-cell foamed aluminum
  • Preparation method of composite material of epoxy resin and closed-cell foamed aluminum
  • Preparation method of composite material of epoxy resin and closed-cell foamed aluminum

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] The first step is the pretreatment of the raw material closed-cell aluminum foam block

[0028] The required amount of raw material closed-cell foamed aluminum blocks of random shape and size remaining from processing, wherein each block contains at least one foam body, and the above-mentioned closed-cell foamed aluminum blocks are treated with 0.1mol / L sodium hydroxide lye The body is degreased and decontaminated, and then treated with 0.01mol / L hydrochloric acid until the lye on the closed-cell aluminum foam block is neutralized to enhance its surface activity and optimize its bonding interface with epoxy resin. Put it into a sealed drying box for use;

[0029] The second step, pretreatment of raw epoxy resin

[0030] Preheat the raw material epoxy resin E-44 and curing agent #651 in a 60°C water bath for 1 hour, then weigh the required amount with a balance, and mix the two according to a mass ratio of 1:1. use;

[0031] The third step, preparation of epoxy resin ...

Embodiment 2

[0039] The first step is the pretreatment of the raw material closed-cell aluminum foam block

[0040] The required amount of raw material closed-cell foamed aluminum blocks of random shape and size remaining from processing, wherein each block contains at least one foam body, and the above-mentioned closed-cell foamed aluminum blocks are treated with 0.1mol / L sodium hydroxide lye The body is degreased and decontaminated, and then treated with 0.01mol / L hydrochloric acid until the lye on the closed-cell aluminum foam block is neutralized to enhance its surface activity and optimize its bonding interface with epoxy resin. Put in a sealed dry box for later use

[0041] The second step, pretreatment of raw epoxy resin

[0042] Preheat the raw material epoxy resin E-44 and curing agent #651 in a 60°C water bath for 1 hour, then weigh the required amount with a balance, and mix the two according to a mass ratio of 1:1. use;

[0043] The third step, preparation of epoxy resin and...

Embodiment 3

[0046] The first step is the pretreatment of the raw material closed-cell aluminum foam block

[0047] Cut the required amount of raw closed-cell aluminum foam into a size of 20×20×20mm 3 The block, with 0.1mol / L sodium hydroxide lye, degrease and decontaminate the above-mentioned closed-cell aluminum foam block, and then treat the alkali on the closed-cell aluminum foam block with 0.01mol / L hydrochloric acid The solution is neutralized to enhance its surface activity and optimize its bonding interface with epoxy resin, and then put it into a sealed dry box for use;

[0048] The second step, pretreatment of raw epoxy resin

[0049] Preheat the raw material epoxy resin E-44 and curing agent #651 in a 60°C water bath for 1 hour, then weigh the required amount with a balance, and mix the two according to a mass ratio of 1:1. use;

[0050] The third step, preparation of epoxy resin and closed-cell aluminum foam composite

[0051] Take out the closed-cell foam aluminum block tr...

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Abstract

The invention discloses a preparation method of a composite material of epoxy resin and closed-cell foamed aluminum, and relates to a composite material which is formed by a high polymer material and a foamed metal material. The preparation method comprises the following steps of: degreasing and decontaminating closed-cell foamed aluminum pieces by using 0.1mol/L of sodium hydroxide alkali liquid; neutralizing the alkali liquid on the closed-cell foamed aluminum pieces by using 0.01mol/L of hydrochloric acid; mixing the epoxy resin E-44 and a curing agent according to a mass ratio of 1:1; proportioning the closed-cell foamed aluminum pieces and the epoxy resin with the curing agent in a mold in a water bath at 70 DEG C according to a volume ratio of 1:1 or 3:1; after bubbles float up, taking out the mold from the water bath; standing for one week at normal temperature so as to obtain a dispersed embedded type epoxy resin and closed-cell foamed aluminum material. By utilizing the method, the defects that the conventional foamed aluminum-based composite material is low in yield strength, resource and energy are wasted in production, the cost is high and the environment can be polluted, are solved.

Description

technical field [0001] The technical solution of the invention relates to a composite material formed of a polymer material and a metal foam material, specifically a preparation method of a composite material of epoxy resin and closed-cell aluminum foam. Background technique [0002] Although the damping performance of polymer materials is better than that of aluminum foam, in terms of mechanical properties, the strength of metal materials is much higher than that of polymer materials. For this reason, the research on metal foam with damping performance has gradually matured in recent years. The research and application of metal foam composite materials with damping properties, especially the research work on aluminum foam composite materials filled with polymer materials has been developed. This kind of composite material composed of aluminum foam filled with polymer phase is expected to combine the advantages of both to obtain a new type of aluminum foam composite material...

Claims

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Application Information

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IPC IPC(8): C08L63/02C08K9/02C08K7/00C08K3/08
Inventor 赵维民安杨夏兴川熊汉青冯辉张欣
Owner TANGSHAN HAODONG PRECISION MACHINERY
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