Preparation method of aescin
A technique for aescin and horse chestnut, which is applied in the field of preparation of aescin, can solve the problems of few medicinal material resources, low content of aescin, troubled scientific researchers and the like
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Embodiment 1
[0018] The invention discloses a preparation method of aescin, which uses the fruit of horse chestnut as a raw material, and undergoes crushing, extraction, concentration, resin adsorption, and elution of impurities to obtain aescin.
[0019] (1) The crushing process is as follows: 2000Kg of horse chestnut fruit is screened out, and then crushed to 10mm particles.
[0020] (2) The extraction process is as follows: add 91% ethanol in three times according to the mass multiple of the horse chestnut fruit, 4 times, and 2 times, and extract three times, that is, add 90% ethanol three times for 8000Kg, 8000Kg, 4000Kg respectively , respectively collected two or three extracts, the extraction time was 2.0h, 2.0h, 2.0h respectively, and the extraction temperature was 80°C, the first extract was concentrated to obtain 20.12% aescin
[0021] (3) The process of concentration is as follows: mix the extracts collected in two or three extractions in the extraction process, and concentrate ...
Embodiment 2
[0028] The invention discloses a preparation method of aescin, which uses the fruit of horse chestnut as a raw material, and undergoes crushing, extraction, concentration, resin adsorption, and elution of impurities to obtain aescin.
[0029] (1) The crushing process is as follows: Screen out 2000Kg of horse chestnut fruit, and then crush it to 15mm particles.
[0030] (2) The extraction process is as follows: add 90% ethanol in three times according to the mass multiple of the horse chestnut fruit, 3.5 times, 3.5 times, and 3 times, and extract three times, that is, add 85% ethanol three times for 7000Kg, 7000Kg, 6000Kg respectively , respectively collect two or three extracts, the extraction time is 2.0h, 1.5h, 1.5h, the extraction temperature is 76°C, 76°C, 85°C respectively, the first extract is concentrated to obtain 20.05% aescin
[0031] (3) The process of concentration is as follows: mix the extracts collected in two or three extractions in the extraction process, and ...
Embodiment 3
[0038] The invention discloses a preparation method of aescin, which uses the fruit of horse chestnut as a raw material, and undergoes crushing, extraction, concentration, resin adsorption, and elution of impurities to obtain aescin.
[0039] (1) The crushing process is as follows: 2000Kg of horse chestnut fruit is screened out, and then crushed to 5mm particles.
[0040] (2) The extraction process is as follows: add 92% ethanol in three times according to the mass multiple of the horse chestnut fruit, 5 times, 3 times, and 2 times, and extract three times, that is, adding 92% ethanol three times is 10000Kg, 6000Kg, 4000Kg respectively , respectively collected two or three extracts, the extraction time was 2.5h, 2.0h, 1.5h, the extraction temperature was 80°C, 80°C, 85°C respectively, the first extract was concentrated to obtain 21.91% aescin
[0041] (3) The process of concentration is as follows: mix the extracts collected from two or three extractions in the extraction proc...
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