First-time charging forming method for lithium-ion secondary battery
A technology of secondary battery and chemical formation method, applied in secondary battery charging/discharging, secondary battery repair/maintenance, non-aqueous electrolyte storage battery, etc., to ensure cycle life and safety performance, improve cycle performance, and avoid negative electrode lithium precipitation Effect
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[0018] Embodiment 1, the first charging formation method of a lithium ion secondary battery provided in this embodiment includes the following steps: the first step, the lithium ion secondary battery that has been filled with electrolyte is heated at a temperature of 20° C. and a relative humidity. It is aged for 12h in an environment of less than or equal to 10%, and then under a negative pressure of -0.085MPa, first charge to 2.5V at a rate of 0.01C, and then charge it to 3.2V at a rate of 0.05C. Then charge to 3.6V with a constant current rate of 0.1C, and seal the battery when the voltage reaches 3.6V.
[0019] In the second step, the sealed battery was aged at 50°C for 24 hours, then charged to 4.0V with a constant current of 0.5C, then charged to 4.2V with a constant current of 0.2C, and finally charged to 4.2V. Under constant voltage charging, the charging cut-off current is 100mA.
Example Embodiment
[0020] Embodiment 2, this embodiment provides a method for forming a lithium ion secondary battery for the first time, including the following steps: the first step, the lithium ion secondary battery that has been filled with electrolyte is heated at a temperature of 70° C. and a relative humidity. It is aged for 24h in an environment of less than or equal to 10%, and then under a negative pressure of -0.092MPa, first charge to 2.5V with a constant current rate of 0.02C, and then charge it to 3.2V with a constant current rate of 0.07C. Then charge to 3.6V with a constant current rate of 0.15C, and seal the battery when the voltage reaches 3.6V.
[0021] In the second step, the sealed battery was aged at 70°C for 72h, then charged to 3.9V with a constant current of 0.7C, then charged to 4.2V with a constant current of 0.3C, and finally charged to 4.2V. Under constant voltage charging, the charging cut-off current is 10mA.
Example Embodiment
[0022] Embodiment 3, the first charging formation method of a lithium ion secondary battery provided in this embodiment includes the following steps. It is aged for 18h in an environment of less than or equal to 3%, and then under a negative pressure of -0.090MPa, first charge to 2.5V with a constant current rate of 0.03C, and then charge it to 3.2V with a constant current rate of 0.1C. Then charge to 3.6V with a constant current rate of 0.2C, and seal the battery when the voltage reaches 3.6V.
[0023] In the second step, the sealed battery was aged at 10°C for 48 hours, and then charged to 3.8V with a constant current of 1C, then charged to 4.2V with a constant current of 0.5C, and finally charged to 4.2V. Constant voltage charging, the charging cut-off current is 200mA.
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