Ferrum-based amorphous soft magnetic material and preparation method thereof
A soft magnetic material, iron-based amorphous technology, applied in the direction of magnetic materials, magnetic objects, electrical components, etc., can solve the problems of decreased amorphous formation ability, decreased maximum saturation magnetic induction intensity, unsatisfactory, etc., to achieve low coercive force , large amorphous formation ability, and the effect of high initial permeability
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[0035] Example 1
[0036] Fe-based amorphous soft magnetic material Fe 77 Y 1 Si 9 B 13 The preparation method specifically includes the following steps:
[0037] Step 1: According to the composition of the iron-based amorphous soft magnetic material, that is, the atomic percentage content, the ingredients are mixed and weighed for use;
[0038] Step 2: First press the high purity Fe, high purity B, and high purity Si as Fe 91.18 -B 8.82 (91.18, 8.82 are mass percentages) and / or Fe 79.91 -Si 20.09 (79.91 and 20.09 are mass percentages) Preparation of master alloy:
[0039] Vacuum the vacuum chamber of the vacuum induction furnace to 5×10 -3 Below Pa, fill with high-purity argon (purity greater than 99.99%) to clean twice, and then smelt the master alloy under the protection of high-purity argon (the melting point temperature range of Fe-B master alloy is (1300~1500) ℃, Fe- The melting point temperature range of Si master alloy is (1200~1400)℃), in order to ensure the uniformity of the...
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[0043] Example 2
[0044] Fe-based amorphous soft magnetic material Fe 76 Y 2 Si 9 B 13 The preparation method specifically includes the following steps:
[0045] Step 1: According to the composition of the iron-based amorphous soft magnetic material, that is, the atomic percentage content, the ingredients are mixed and weighed for use;
[0046] Step 2: First press the high purity Fe, high purity B, and high purity Si as Fe 91.18 -B 8.82 (91.18, 8.82 are mass percentages) and / or Fe 79.91 -Si 20.09 (79.91 and 20.09 are mass percentages) Preparation of master alloy:
[0047] Vacuum the vacuum chamber of the vacuum induction furnace to 5×10 -3 Below Pa, fill with high-purity argon (purity greater than 99.99%) to clean twice, and then smelt the master alloy under the protection of high-purity argon (the melting point temperature range of Fe-B master alloy is (1300~1500) ℃, Fe- The melting point temperature range of Si master alloy is (1200 ~ 1400) ℃), in order to ensure the uniformity of ...
Example Embodiment
[0055] Example 3
[0056] Fe-based amorphous soft magnetic material Fe 75 Y 3 Si 9 B 13 The preparation method specifically includes the following steps:
[0057] Step 1: According to the composition of the iron-based amorphous soft magnetic material, that is, the atomic percentage content, the ingredients are mixed and weighed for use;
[0058] Step 2: First, prepare high-purity Fe, high-purity B, and high-purity Si as Fe-B and / or Fe-Si master alloys, where Fe-B master alloy B is 7wt.%, Fe-Si master alloy Si is 15wt .%:
[0059] Vacuum the vacuum chamber of the vacuum arc furnace to 5×10 -3 Below Pa, fill with high-purity argon (purity greater than 99.99%) to clean twice, and then smelt the master alloy under the protection of high-purity argon (the melting point temperature range of Fe-B master alloy is (1300~1500) ℃, Fe- The melting point temperature range of Si master alloy is (1200~1400) ℃), in order to ensure the uniformity of the composition, it is repeatedly smelted 3 to 5 ti...
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