Rapid drying screen clogging resistance composition for aqueous coating material screen printing, and preparation method thereof
A technology of screen printing and water-based paint, applied in dyeing method, textile and papermaking, etc., can solve the problems of affecting the printability of printing paint, thickening of printing paint, prolonging the drying time of imprinting, etc., to improve printing production efficiency, prevent The effect of blocking the net phenomenon and shortening the drying time
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Embodiment 1
[0026] The synthesis of embodiment 1 water-soluble copolymer solution
[0027] Add 24.71g of acrylamide, 4.36g of acrylic acid and 461.2g of soft water into a 1000mL four-necked flask with stirring, start stirring, heat to 40°C, then add 10mL of 1.0% by mass ammonium persulfate aqueous solution, gradually Raise the temperature to 80°C, react at this temperature for 3 minutes, then add the mixed monomer solution consisting of 74.12g acrylamide, 13.08g acrylic acid and 147.7g soft water through the dropping funnel at a constant speed, and add it within 1 hour, and add it simultaneously and at a uniform speed 40mL of ammonium persulfate aqueous solution with a mass percentage of 1.0% was stirred and reacted at 80°C for 1 hour, and discharged while hot to obtain a water-soluble acrylamide-acrylic acid copolymer solution with a solid content of 15%. The viscosity (25°C ) 2.50×10 3 mPa·s, the mass composition ratio of the copolymer molecule is: acrylamide component 85%, acrylic a...
Embodiment 2
[0028] The synthesis of embodiment 2 water-soluble copolymer solution
[0029] In a stirred 1000mL four-neck flask, add 25.28g of acrylamide, 2.81g of acrylic acid and 418.5g of soft water, start stirring, heat to 40°C, then add 10mL of 0.95% by mass ammonium persulfate aqueous solution, gradually Raise the temperature to 84°C, react at this temperature for 3 minutes, and then uniformly add the mixed monomer solution consisting of 78.82g acrylamide, 8.42g acrylic acid and 168.0g soft water through the dropping funnel. 40mL 0.95% ammonium persulfate aqueous solution. Continue to stir and react at 84°C for 1 hour, discharge while hot to obtain a water-soluble acrylamide-acrylic acid copolymer aqueous solution with a solid content of 15%, viscosity (25°C) 2.45×10 3 mPa s. The mass composition ratio of the copolymer molecule is: 90% of the acrylamide component and 10% of the acrylic component.
Embodiment 3
[0030] The synthesis of embodiment 3 water-soluble copolymer solution
[0031] Add 21.81g of acrylamide, 7.27g of acrylic acid and 302.4g of soft water into a 1000mL four-necked flask with stirring, start stirring, heat to 45°C, then add 12mL of 0.90% by mass ammonium persulfate aqueous solution, gradually Raise the temperature to 75°C, react at this temperature for 5 minutes, and then uniformly add the mixed monomer solution consisting of 65.40g acrylamide, 21.81g acrylic acid and 110.8g soft water through the dropping funnel. 40mL 0.90% ammonium persulfate aqueous solution by mass. Then continue to stir and react at 75°C for 1 hour, discharge while hot to obtain a water-soluble acrylamide-acrylic acid copolymer aqueous solution with a solid content of 20%, viscosity (25°C) 8.23×10 3 mPa s. The mass composition ratio of the copolymer molecule is: 75.0% of acrylamide component and 25.0% of acrylic acid component.
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