A kind of ammonia storage active mixture sample block with rich pores and preparation method thereof
A technology of active mixture and mixture, which is applied in the field of ammonia-storage active mixture samples with rich channels and its preparation, can solve the problems of lack of clear claim details and technical personnel's inability to implement, and achieve the effect of meeting the requirements of use
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Embodiment 1
[0012] 73wt% industrial anhydrous strontium chloride salt powder, 8wt% sucrose, 5wt% molecular sieve and 14wt% industrial alcohol are used to form a mixture; the mixture is stirred evenly by a mixer for 1 hour to form a semi-dry mixed powder; The semi-dry mixed powder is added into an openable airtight container and mechanically shaken for 30 minutes to form a wet sample block; the sample block is sintered at 350°C for 4 hours to obtain a solid sample of the ammonia storage mixture containing amorphous carbon piece.
[0013] Fill the 10g solid sample block with ammonia in a naturally ventilated environment. Put the openable airtight container into a water tank with enough cooling water in advance, connect the ammonia steel cylinder, and pass through the pressure reducing valve and drying system. Ammonia charging is carried out slowly within the pressure range of 0.4Mpa, and the ammonia charging time is 5 hours; after ammonia charging, the mass of the sample block is 14.2g, tha...
Embodiment 2
[0015] 81wt% industrial anhydrous strontium chloride salt powder, 3wt% sucrose, 5wt% molecular sieve and 11wt% industrial alcohol are used to form a mixture; the mixture is stirred evenly by a mixer for 5 hours to form a semi-dry mixed powder; The semi-dry mixed powder is added into an openable airtight container and mechanically shaken for 30 minutes to form a wet sample block; the sample block is sintered at 450°C for 3 hours to obtain a solid sample of the ammonia storage mixture containing amorphous carbon piece.
[0016] Fill the 10g solid sample block with ammonia in a naturally ventilated environment. Put the openable airtight container into a water tank with enough cooling water in advance, connect the ammonia steel cylinder, and pass through the pressure reducing valve and drying system. Charge ammonia slowly within the pressure range of 0.3Mpa, and the ammonia charging time is 5 hours; after ammonia charging, the mass of the sample block is 14.6g, that is, 4.6g of am...
Embodiment 3
[0018] 69wt% industrial anhydrous strontium chloride salt powder, 11wt% sucrose, 10wt% molecular sieve and 10wt% industrial alcohol are used to form a mixture; the mixture is stirred evenly by a mixer for 10 hours to form a semi-dry mixed powder; The semi-dry mixed powder is added into an openable airtight container and mechanically shaken for 40 minutes to form a wet sample block; the sample block is sintered at 400°C for 5 hours to obtain a solid sample of the ammonia storage mixture containing amorphous carbon piece.
[0019] Fill the 10g solid sample block with ammonia in a naturally ventilated environment. Put the openable airtight container into a water tank with enough cooling water in advance, connect the ammonia steel cylinder, and pass through the pressure reducing valve and drying system. Charge ammonia slowly within the pressure range of 0.4Mpa, and the ammonia charging time is 4 hours; after ammonia charging, the mass of the sample block is 13.8g, that is, 3.8g of...
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