Porous solid sample block of ammonia storage active mixture containing industrial clay and preparation method thereof
A technology of active mixtures and porous solids, applied in the direction of ammonia compounds, silicon compounds, alkali metal compounds, etc., can solve the problems that technical personnel cannot implement, have no dosage ratio, and have no clear claim details, etc., to increase the number of macroscopic pores , improve the adsorption characteristics and meet the requirements of use
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Embodiment 1
[0015] 36wt% industrial anhydrous strontium chloride salt powder, 24wt% industrial clay, 2wt% high specific surface area activated carbon, 12wt% deionized water and 26wt% industrial alcohol form a mixture, which is stirred evenly by a mixer, and the stirring time is After 1 hour, a semi-dry mixed powder is formed; the powder is added into an openable airtight container, subjected to mechanical vibration for 30 minutes, and then dried at 80°C for 1 hour under the condition of a vacuum of 1Kpa to obtain a content of 38.7 Porous solid samples of ammonia storage active mixture of wt% clay for industrial use.
[0016] Fill the 10g porous solid sample block with ammonia in a naturally ventilated environment. Put the openable airtight container in a water tank with enough cooling water in advance, connect the ammonia cylinder, and pass through the pressure reducing valve and the drying system. , fill ammonia slowly within the pressure range of 0.6Mpa, and the ammonia filling time is ...
Embodiment 2
[0018] 80wt% of industrial anhydrous strontium chloride salt powder, 4wt% of industrial clay, 7wt% of high specific surface area activated carbon, 4wt% of deionized water and 5wt% of industrial alcohol form a mixture, which is stirred evenly by a mixer, and the stirring time is After 5 hours, a semi-dry mixed powder is formed; the powder is added to an openable airtight container and mechanically shaken for 60 minutes, and then at 60°C, the vacuum degree is 10 -1 Under the condition of Kpa, dry for 3h, you can get the porous solid sample block of ammonia storage active mixture containing 4.3wt% industrial clay 。
[0019] Fill the 10g porous solid sample block with ammonia in a naturally ventilated environment. Put the openable airtight container in a water tank with enough cooling water in advance, connect the ammonia cylinder, and pass through the pressure reducing valve and the drying system. , fill the ammonia slowly within the pressure range of 0.1Mpa, the ammonia filling...
Embodiment 3
[0021] 70wt% of industrial anhydrous strontium chloride salt powder, 15wt% of industrial clay, 5wt% of high specific surface area activated carbon, 5wt% of deionized water and 5wt% of industrial alcohol form a mixture, which is stirred evenly by a mixer, and the stirring time is After 10 hours, a semi-dry mixed powder was formed; the powder was added into an openable airtight container, mechanically shaken for 60 minutes, and then dried for 3 hours at a temperature of 100°C to obtain a powder containing 16.7wt% industrial clay. Ammonia storage active mixture porous solid sample block 。
[0022] Fill the 10g porous solid sample block with ammonia in a naturally ventilated environment. Put the openable airtight container in a water tank with enough cooling water in advance, connect the ammonia cylinder, and pass through the pressure reducing valve and the drying system. , fill ammonia slowly within the pressure range of 0.4Mpa, and the ammonia filling time is 5h; after ammonia ...
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