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Calcium carbide particles, method for producing calcium carbide particles, and system for producing calcium carbide particles

A technology of particle manufacturing and calcium carbide, which is applied in the direction of calcium carbide and carbide

Active Publication Date: 2016-04-13
DENKA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition, although the carbide is conveyed to the raw material airtight tank by the screw conveyor, another screw conveyor is required to return the carbide overflowing from the raw material airtight tank to the intermediate tank

Method used

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  • Calcium carbide particles, method for producing calcium carbide particles, and system for producing calcium carbide particles
  • Calcium carbide particles, method for producing calcium carbide particles, and system for producing calcium carbide particles
  • Calcium carbide particles, method for producing calcium carbide particles, and system for producing calcium carbide particles

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] For the above-mentioned pulverizer 20, the gap of the upper segment between the striking plate 22a of the rotor 22 and the crushing liner 23a of the crushing plate 23 is set to 50 mm, the gap of the lower segment is set to 30 mm, and the rotating speed of the rotor 22 is set to 45 m / s (650rpm), the carbide is fed from the supply port 21a at 40t / h. The amount of carbides passed through the sieve 30 after pulverization by the pulverizer 20 was 15 t / h, and the circulation ratio was (40−15) / 15=about 1.7. Table 1 shows the particle size distribution (mass basis) of the carbide particles (passed through the sieve 30 ) obtained by operating the pulverizer 20 for a long time at this circulation ratio.

[0030] [Table 1]

[0031] Sieve hole (mm)

4.75 or more

4.0 or above

4.0~3.0

3.0~2.0

2.0~1.0

1.0~0.5

0.5~0.15

Below 0.15

Ratio (%)

0.0

0.2

13.5

17.4

25.2

15.0

22.6

6.2

[0032] Average parti...

Embodiment 2

[0057] For the pulverizer 20, the gap of the upper section between the striking plate 22a of the rotor 22 and the crushing liner 23a of the crushing plate 23 is set to 55mm, the gap of the lower section is set to 32mm, and the rotating speed of the rotor 22 is set to 45m / s ( 650rpm), carbides were fed from the supply port 21a at a rate of 52.5t / h. The amount of carbides that passed through the sieve 30 after pulverization by the pulverizer 20 was 15 t / h, and the circulation ratio was (52.5−15) / 15=2.5. Table 4 shows the particle size distribution (mass basis) of the carbide particles (passed through the sieve 30 ) obtained by operating the pulverizer 20 for a long time at this circulation ratio.

[0058] [Table 4]

[0059] Sieve hole (mm)

4.75 or more

4.0 or above

4.0~3.0

3.0~2.0

2.0~1.0

1.0~0.5

0.5~0.15

Below 0.15

Ratio (%)

1.2

3.8

21.7

18.8

21.5

15.4

14.1

3.5

[0060] Average particle siz...

Embodiment 3

[0066] For the pulverizer 20, the gap of the upper segment between the striking plate 22a of the rotor 22 and the crushing liner 23a of the crushing plate 23 is set as 45mm, the gap of the lower segment is set as 22mm, and the rotating speed of the rotor 22 is set as 45m / s ( 650rpm), carbides were fed from the supply port 21a at a rate of 30t / h. The amount of carbides that passed through the sieve 30 after pulverization by the pulverizer 20 was 15 t / h, and the circulation ratio was (30−15) / 15=1.0. Table 5 shows the particle size distribution (mass basis) of the carbide particles (passed through the sieve 30 ) obtained by operating the pulverizer 20 for a long time at this circulation ratio.

[0067] [table 5]

[0068] Sieve hole (mm)

4.75 or more

4.0 or above

4.0~3.0

3.0~2.0

2.0~1.0

1.0~0.5

0.5~0.15

Below 0.15

Ratio (%)

0.0

0.1

6.3

15.5

19.7

21.1

17.3

20.0

[0069] Average particle size: 0...

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Abstract

Provided is a process for producing calcium carbide granules which, when used for dry-process acetylene generation, neither enhance side reactions such as acetylene polymerization, nor adversely affect the yield, nor enhance the risk to safety due to an increase in reaction temperature. The process is for producing calcium carbide granules in which the content of granules having a diameter of 4 mm or larger is 5 wt.% or less and the content of granules having a diameter of 0.15 mm or smaller is 20 wt.% or less, the process comprising the step (A) of crushing calcium carbide with a crusher, the step (B) of putting the calcium carbide which has been crushed with the crusher through a screen having an opening size of 4 mm, and the step (C) of introducing the calcium carbide remaining on the screen into the crusher again. The steps (A) to (C) are conducted in an inert gas atmosphere. The size of crushed granules to be obtained by the crusher is controlled so that the amount of the calcium carbide introduced into the crusher in the step (A), a, and the amount of the calcium carbide passing through the screen in the step (B), b, satisfy 1‰¤(a-b) / b‰¤2.5.

Description

technical field [0001] The present invention relates to calcium carbide particles, a method for producing calcium carbide particles and a system for producing calcium carbide particles, more specifically, calcium carbide particles suitable for dry acetylene generation, and a method and system for producing such calcium carbide particles. Background technique [0002] When calcium carbide (hereinafter referred to simply as "carbide") is supplied to the acetylene generator for dry acetylene generation, the carbide block is preliminarily crushed, and the carbide is introduced into a pulverizer for fine pulverization. The carbide is conveyed to the raw material sealed tank above the acetylene generator. The smaller the particle size of the carbide, the higher the reactivity when acetylene is generated, and the higher the sealing function of the carbide tightly accommodated in the raw material sealed tank to prevent acetylene gas from flowing into the raw material sealed tank. T...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B31/32C07C11/24C01B32/942
CPCC01B32/942
Inventor 谷村恭一镰本隼平窪野孝治大森博昭长崎俊一
Owner DENKA CO LTD