Acrylamide monomer and its preparation method and acrylamide copolymer and its preparation method and application
A technology of acrylamide copolymer and acrylamide copolymerization, which is applied in the direction of sulfonic acid preparation, drilling composition, chemical instruments and methods, etc., can solve the problems of poor temperature and salt resistance, and achieve not easy curling and improved salt resistance Performance, large volume effect
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Embodiment 1
[0093] This example is used to illustrate the acrylamide monomer and acrylamide copolymer provided by the present invention and its preparation method
[0094] (1) Preparation of acrylamide monomer
[0095] Add 100 kg of concentrated sulfuric acid with a weight concentration of 98% into the reaction kettle, add 530 kg of acrylonitrile, cool the mixture to -5°C, stir evenly, add 104.14 kg of styrene, and keep the temperature of the reaction system below 5°C. Continue to stir the reaction for 2h, static, and crystals are precipitated. After filtering, washing, refining and drying, the pure monomer was obtained, and the product yield was 95.5%, and the acrylamide monomer M1 was obtained.
[0096] (2) Preparation of acrylamide copolymer
[0097] Add 927.09 kg of acrylamide (AM) and 831.46 kg of acrylamide monomer M1, and 7034.2 kg of deionized water into the batching kettle. While stirring, use frozen brine to control the solution temperature -7°C, and add sodium hydroxide to ad...
Embodiment 2
[0101] This example is used to illustrate the acrylamide monomer and acrylamide copolymer provided by the present invention and the preparation method thereof.
[0102] (1) Preparation of acrylamide monomer
[0103] Add 117.6 kg of concentrated sulfuric acid with a weight concentration of 98% to the reaction kettle, add 1060 kg of acrylonitrile, cool the mixture to 15°C, stir evenly, add 104.14 kg of styrene, and keep the temperature of the reaction system below 5°C. Continue to stir the reaction for 4h, static, and crystals are precipitated. After filtering, washing, refining and drying, the pure monomer was obtained, and the product yield was 96%, and the acrylamide monomer M2 was obtained.
[0104] (2) Preparation of acrylamide copolymer
[0105] Add 1108.85 kg of AM, 102.00 kg of acrylamide monomer M2, and 2825.3 kg of deionized water into the batching kettle. While stirring, control the temperature of the solution with frozen brine to 15°C, and add sodium hydroxide to a...
Embodiment 3
[0107] This example is used to illustrate the acrylamide monomer and acrylamide copolymer provided by the present invention and the preparation method thereof.
[0108] (1) Preparation of acrylamide monomer
[0109] Add 107.8 kg of concentrated sulfuric acid with a weight concentration of 98% to the reaction kettle, add 636 kg of acrylonitrile, cool the mixture to 5°C, stir evenly, add 104.14 kg of styrene, and keep the temperature of the reaction system below 5°C. Continue to stir the reaction for 3h, static, and crystals are precipitated. After filtering, washing, refining and drying, the pure monomer was obtained, and the product yield was 97%, and the acrylamide monomer M3 was obtained.
[0110] (2) Preparation of acrylamide copolymer
[0111] Add 1,080.4 kg of AM, 204.0 kg of temperature-resistant and salt-resistant monomer M3, and 3,853.2 kg of deionized water into the batching kettle. While stirring, use frozen brine to control the solution temperature at 0°C, and add...
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