Upstroke reaction steam stripping separator and hydrogenation method

A technology of stripping separation and reaction zone, which is applied in the fields of hydrogenation treatment process, petroleum industry, and hydrocarbon oil treatment. It can solve the problems of many equipment leakage points, large equipment investment and floor space, and hidden safety hazards, and achieves a simple structure. , Small footprint, high safety effect

Active Publication Date: 2014-06-04
CHINA PETROCHEMICAL CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] However, at present, the upward reactor and the stripper mass transfer separator are two independent devices, and the equipment investment

Method used

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  • Upstroke reaction steam stripping separator and hydrogenation method
  • Upstroke reaction steam stripping separator and hydrogenation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0038] Such as figure 1 Shown, an upward reactive stripping separator. Including: reaction zone and mass transfer separation zone,

[0039] The reaction zone and the mass transfer separation zone are placed in the same container shell 1, the reaction zone is set in the lower part, the mass transfer separation zone is set in the upper part, and an annular intermediate partition plate 2 is arranged between the reaction zone and the mass transfer separation zone and the manhole channel 3, the middle partition plate 2, the manhole channel 3 and the container shell 1 form an annular space with the lower end closed and the upper end open, and the mass transfer separation zone is in the annular space;

[0040] An upward fixed-bed catalyst bed 7 is filled in the reaction zone, and an annular tray 14 is filled in the mass transfer separation zone;

[0041] The bottom of the container is provided with a reaction raw material inlet 4, and the top of the container is provided with a gas...

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PUM

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Abstract

The invention discloses an upstroke reaction steam stripping separator and a hydrogenation method. The reaction steam stripping separator comprises a reaction zone and a mass transfer separation zone, the reaction zone and the mass transfer separation zone are arranged in a same container shell body, the reaction zone is arranged in the lower part, the mass transfer separation zone is arranged in the upper part, an annular middle spacer plate and a manhole passage are arranged between the reaction zone and the mass transfer separation zone, an annular space is formed by the middle spacer plate, manhole passage and container shell body, and the annular space is closed at the lower end and is provided with an opening at the upper end, and the mass transfer separation zone is in the annular space. The method is as follows: raw material oil and a part of hydrogen enter from the bottom of the upstroke reaction steam stripping separator, the other part of the hydrogen is injected from reaction zone catalyst bed interlamination for hydrogenation reaction in a reaction zone, a gas phase product is collected at the top, and a liquid phase product is collected at the side wall. According to the upstroke reaction steam stripping separator and the hydrogenation method, equipment investment and occupied area are reduced, the problem that many leakage points are produced for the reason that two independent equipment are connected by pipelines is reduced, and the device safety is improved.

Description

technical field [0001] The invention relates to the field of hydrogenation reaction, and more particularly, relates to an upward reaction stripping separator and a hydrogenation method. Background technique [0002] In the field of petrochemical hydrogenation, independent fixed-bed reactors and stripper mass transfer separators are often installed. The fixed-bed reactors usually adopt a downward type, that is, the raw materials enter from the top of the reactor, and the reaction products flow out from the bottom of the reactor. The reaction product then enters a separate stripping tower for stripping and mass transfer separation of gas phase products and liquid phase products. [0003] When adopting the scheme of the ascending reactor, the raw material enters from the bottom of the reactor, and the reaction product flows out from the top of the reactor. Since the flow direction of the gas in the upward reactor is consistent with the diffusion direction of the gas, the possi...

Claims

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Application Information

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IPC IPC(8): C10G67/04
Inventor 刘凯祥刘家明王鹤李浩孙丽丽
Owner CHINA PETROCHEMICAL CORP
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