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Preparation method of intermediate-temperature magnesium strengthening porcelain and product prepared from intermediate-temperature magnesium strengthening porcelain

A technology of strengthening porcelain and medium temperature, which is applied in the field of preparation of medium temperature magnesia strengthening porcelain, which can solve the problems that hinder the quality of medium temperature magnesia daily-use ceramics, narrow firing temperature range, and easy to produce pinhole defects, etc., and achieve the elimination of glaze pinholes. hole, eliminate residual stress, good glaze quality effect

Active Publication Date: 2014-09-03
JIANGXI GALOBAL CERAMIC CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, most of the preparation methods of domestic medium-temperature magnesia reinforced porcelain adopt a one-time firing process. However, due to the narrow firing temperature range of magnesia porcelain, it is difficult to control the temperature during the firing process. When the temperature is too high or the holding time is too long, deformation defects are easy to occur. , when the temperature is too low or the holding time is short, it is easy to produce cracking defects. Therefore, in the current production process of medium-temperature magnesia reinforced porcelain, in order to widen the firing range, about 30% raw talc is often added. However, due to the one-time firing process, During the firing process, more pinhole defects will be produced on the glaze surface due to the decomposition of raw talc. In addition, because the expansion coefficient of the magnesia reinforced porcelain body is relatively large, the expansion coefficient of the glaze must match it. The surface gloss is poor and pinhole defects are prone to occur. Therefore, the current preparation methods of medium-temperature magnesia reinforced porcelain can no longer meet the needs of consumers, which seriously hinders the improvement of the quality of medium-temperature magnesia daily-use ceramics

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A medium-temperature magnesia reinforced porcelain. The blank is weighed according to the mass percentage: 32% burnt talc, 26% raw talc, 10% feldspar, 15% kaolin, 4% bentonite, and 13% quartz. After mixing and ball milling, the grinding mud is controlled. The fineness of the material is 0.008% and the remainder of the sieve with 10,000 holes. After the mud is stale, the green body is obtained by grouting. The green body has been bisque-fired in advance. The biscuit firing temperature is 1250 ° C and the holding time is 30 minutes;

[0020] Weigh the glaze by mass percentage: feldspar 24%, calcite 14%, kaolin 6%, quartz 14%, ZnO3%, BaCO 3 4%, glass frit 35%, after mixing and ball milling, the fineness of the grinding mud is controlled to be 0.03% and the remainder of the million-hole sieve, and then glazed on the inner and outer surfaces of the biscuit-fired plain tire, dried, fired at 1100°C, and the holding time for 30min.

[0021] The prepared sample was tested for g...

Embodiment 2

[0023] A medium-temperature magnesia reinforced porcelain. The blank is weighed according to the mass percentage: 40% burnt talc, 22% raw talc, 8% feldspar, 11% kaolin, 5% bentonite, and 14% quartz. After mixing and ball milling, the grinding mud is controlled. The fineness of the material is 0.008% and the remainder of the sieve with 10,000 holes. After the mud is stale, the green body is obtained by grouting. The green body has been bisque-fired in advance. The biscuit firing temperature is 1250 ° C and the holding time is 30 minutes;

[0024] Weigh the glaze by mass percentage: 34% feldspar, 11% calcite, 8% kaolin, 12% quartz, ZnO5%, BaCO 3 5%, glass frit 25%, through mixing and ball milling, the fineness of the grinding mud is controlled to be 0.03% and the remainder of the million-hole sieve, and then glazed on the inner and outer surfaces of the plain fired plain tire, dried, fired at 1100°C, and the holding time for 30min.

[0025] The prepared sample was tested for gl...

Embodiment 3

[0027] A medium-temperature magnesia reinforced porcelain. The blank is weighed according to the mass percentage: 44% burnt talc, 33% raw talc, 5% feldspar, 13% kaolin, 3% bentonite, and 2% quartz. After mixing and ball milling, the grinding mud is controlled. The fineness of the material is 0.008% and the remainder of the sieve with 10,000 holes. After the mud is stale, the green body is obtained by grouting. The green body has been bisque-fired in advance. The biscuit firing temperature is 1250 ° C and the holding time is 30 minutes;

[0028] Weigh the glaze by mass percentage: feldspar 40%, calcite 7%, kaolin 8%, quartz 5%, ZnO5%, BaCO 3 5%, glass frit 30%, through mixing and ball milling, the fineness of the grinding mud is controlled to be 0.03% and the remainder of the million-hole sieve, and then glazed on the inner and outer surfaces of the plain-fired plain tire, dried, fired at 1100 ° C, and the holding time for 30min.

[0029] The prepared sample was tested for glo...

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Abstract

The invention relates to a preparation method of an intermediate-temperature magnesium strengthening porcelain and a product prepared from the intermediate-temperature magnesium strengthening porcelain. The formula of the strengthening porcelain comprises the following billet materials and glaze materials by weight percent: the billet materials: 30% to 45% of sintered talc, 20% to 35% of raw talc, 5% to 15% of feldspar, 10% to 18% of kaolin, 3% to 5% of bentonite and 0% to 15% of quartz; the glaze materials: 20% to 40% of feldspar, 5% to 15% of calcite, 4% to 8% of kaolin, 0% to 15% of quartz, 3% to 5% of ZnO, 3% to 5% of BaCO and 20% to 35% of glass materials. The preparation method comprises the following steps: carrying preparation, molding, drying, billet biscuiting, glazing, drying and intermediate-temperature glaze firing on the billet materials and the glaze materials under the conditions that the biscuiting temperature of a billet is controlled within 1240 DEG C to 1260 DEG C, the heat preservation time of the billet is 30 minutes, the firing time of an intermediate-temperature glaze is 1100 DEG C and the firing time of the intermediate-temperature glaze is 30 minutes, thereby obtaining the strengthening porcelain with a good glaze surface quality and a high glossiness. Thus, the method has a wide application prospect.

Description

technical field [0001] The invention belongs to the field of inorganic non-metallic materials (ceramics), and in particular relates to a preparation method of medium-temperature magnesia reinforced porcelain and a prepared product thereof. Background technique [0002] At present, most of the preparation methods of domestic medium-temperature magnesia reinforced porcelain adopt a one-time firing process. However, due to the narrow firing temperature range of magnesia porcelain, it is difficult to control the temperature during the firing process. When the temperature is too high or the holding time is too long, deformation defects are easy to occur. , when the temperature is too low or the holding time is short, it is easy to produce cracking defects. Therefore, in the current production process of medium-temperature magnesia reinforced porcelain, in order to widen the firing range, about 30% raw talc is often added. However, due to the one-time firing process, During the fi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/16C04B41/86
Inventor 徐金昌刘文辉潘发旺
Owner JIANGXI GALOBAL CERAMIC CO LTD
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