Qiama ancient glucosinolate extract and its preparation method
A technology of glucosinolates and glucosinolates of Chamagu, which is applied in the field of glucosinolate extracts of Chamagu and their preparation, can solve the problems of low yield of glucosinolates, can not meet the requirements of industrialized production and the like, and achieves the yield High, improve the effect of extraction efficiency
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Embodiment 1
[0022] Example 1, the Qiamagu glucosinolate extract is obtained according to the following preparation method: in the first step, the raw material Qiamagu is washed and pulverized, and then vacuum-dried to obtain dry Qiamagu, and 1 gram of dry Qiamagu Add 7ml to 11ml of methanol aqueous solution with a volume percentage of 80% to 100%, add methanol aqueous solution to the dried Chamagu, and perform one extraction in a constant temperature water bath at a temperature of 80°C for 0.5 hours to 1.5 hours. After the separation, the primary extract and the primary residue are obtained; the second step is to add an 80% to 100% methanol aqueous solution equal to the volume percentage of the first step to the primary residue, and place it in a constant temperature water bath at 80°C for 0.5 hours Carry out the secondary extraction for 1.5 hours, and obtain the secondary extraction solution and the secondary residue after the secondary extraction and separation; the third step, mix the p...
Embodiment 2
[0023] Example 2, the Qiamagu glucosinolate extract is obtained according to the following preparation method: in the first step, the raw material Qiamagu is washed and pulverized, and then vacuum-dried to obtain dry Qiamagu, and 1 gram of dry Qiamagu Add 7 milliliters or 11 milliliters of 80% or 100% methanol aqueous solution to the dry Qiamagu, add methanol aqueous solution to the dry Qiamagu, and perform an extraction once in a constant temperature water bath at a temperature of 80 ° C for 0.5 hours or 1.5 hours. After the separation, the primary extract and the primary residue are obtained; in the second step, an 80% or 100% methanol aqueous solution equal to the volume percentage of the first step is added to the primary residue, and the temperature is 80°C in a constant temperature water bath for 0.5 hours Or carry out secondary extraction in 1.5 hours, obtain secondary extraction solution and secondary residue after secondary extraction and separation; third step, mix pr...
Embodiment 3
[0024] Example 3, as an optimization of the above example, in the first step of Example 3, the raw material Qiamagu is crushed to a particle size of 50 mesh to 10 mesh, and then the pulverized raw material Qiamagu is placed at a temperature of 40 °C to 70 °C and vacuum drying at a pressure of -0.06Mpa to -0.09Mpa to obtain dry Chamagu with a mass percentage moisture content of less than or equal to 20%.
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