Application of Mexico artemisin in preparing antitumor drugs
An anti-tumor drug, artemisinin technology, applied in the field of medicine
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Embodiment 1
[0050] Preparation of Mexican artemisinin
[0051] Take 500g of the coarse powder of the aerial part of Artemisia Chrysanthemum, put it in an extraction kettle, add methanol as an entrainer at a solid-to-liquid volume ratio of 5:2, and feed in liquid CO2 at a pressure of 22MPa and a temperature of 38°C, with a CO2 flow rate of 4.5ml / g crude drug / min, extract for 120min, analyze at a pressure of 7MPa and a temperature of 32°C, collect the extract, add 15g of diatomaceous earth to stir for decolorization, filter to obtain a decolorization solution, concentrate to a relative density of 1.12, and put on a neutral alumina column (column pressure is 6bar, column diameter-to-height ratio is 1:8), eluted and purified with petroleum ether-ethyl acetate 3:14, and the crude product of Mexican artemisinin is obtained; the volume ratio is 19:38:45 methanol-acetonitrile-water Mobile phase, the crude product is dissolved in the mobile phase, injected into the preparative high-performance li...
Embodiment 2
[0053] Tablet: 40g of Mexican artemisinin, 135g of starch, 25g of chenodeoxycholate, granulated and compressed into 1000 tablets. Dosage: Adults take 1 tablet at a time, 2 times a day.
Embodiment 3
[0055] Capsules: Mexican artemisinin 40g, starch 135g, chitosan 25g, mix well, and make 1000 capsules. Dosage: Adults take 1 capsule at a time, 2 times a day.
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