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Preparation method for catalyst

A catalyst and catalyst carrier technology, applied in catalyst activation/preparation, chemical instruments and methods, physical/chemical process catalysts, etc., can solve problems such as inability to produce non-uniform catalysts, inability to achieve continuous production, and damage to catalyst carrier structures.

Inactive Publication Date: 2015-02-25
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, although these impregnation equipment can accomplish the purpose of impregnating active components on the catalyst, there are many problems in these impregnation equipment and devices, such as intermittent operation, continuous production cannot be realized, and product quality is not stable, and the throughput Small defects, catalyst support structure damage and other problems
[0004] In addition, many diffusion-limited catalytic reactions and highly exothermic catalytic reactions require heterogeneous catalysts to meet the requirements of the reaction process. Traditional production equipment can no longer meet the requirements of producing heterogeneous catalysts.

Method used

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  • Preparation method for catalyst
  • Preparation method for catalyst

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preparation example Construction

[0036] First, the present invention provides a catalyst preparation method, which is based on the impregnation method, that is, includes an impregnation step, and in the impregnation step, the purpose of impregnating the catalyst with an active component solution is achieved. The shape of the catalyst carrier has various shapes, such as circular, ellipsoid, Raschig ring and other structures. In addition, the active material in the active component solution mainly depends on the type of catalyst, such as various chemical elements such as alum and silver. In order to realize the purpose of the present invention, in the impregnation step of the preparation method provided by the invention, the catalyst carrier and the active component solution containing the active substance can be respectively input into the rotating drum 1 arranged at an inclination, and on the side of the rotating drum 1 The wall is provided with a turning member 11, wherein the active component solution is spr...

Embodiment 1

[0054]1. Put a strip-shaped alumina as a catalyst carrier and put it into the hopper-type carrier storage device 2, and enter the feed hopper 11 of the drum 1 through the second adjustment device 22 and the second conveyor belt 21 for transmission.

[0055] 2. The active component solution in the tank solution storage device 3 is transported through the pumping mechanism 32 first, and the active component in it is Ni+Mo, and then passes through the first regulating device 32 and enters the spray bar 5 and the atomizing nozzle 51 . The atomizing nozzle is a pressure nozzle, which can atomize the solution into droplets with a particle size of 20 microns to 120 microns, and spray them into the drum 1 at a volume flow rate of 0.3QM.

[0056] 3. Drive the rotating drum 1 by the rotating drive device 62, the rotating speed is 5 revolutions per minute, and the inner wall of the rotating drum 1 is provided with a material turning member 11, so that the catalyst carrier can be raised to...

Embodiment 2

[0060] 1. Put a strip-shaped alumina as a catalyst carrier and put it into the hopper-type carrier storage device 2, and enter the feed hopper 11 of the drum 1 through the second adjustment device 22 and the second conveyor belt 21 for transmission.

[0061] 2. The active component solution in the tank-type solution storage device 3 is first transported through the pumping mechanism 32 , and the active component therein is Co, then passes through the first regulating device 32 , and enters the spray bar 5 and the atomizing nozzle 51 . The atomizing nozzle is a pressure nozzle, which can atomize the solution into droplets with a particle size of 30 microns to 100 microns, and spray them into the drum 1 at a flow rate of 0.37 QM.

[0062] 3. Drive the rotating drum 1 by the rotating drive device 62, the rotating speed is 6 revolutions per minute, the inner wall of the rotating drum 1 is provided with a material turning member 11, so that the catalyst carrier can be raised to a ce...

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Abstract

The invention discloses a preparation method for a catalyst, which is characterized in that in a dipping step, a catalyst carrier and a solution containing the active components are respectively input in an aslant arranged rotating cylinder, a material turning piece is arranged on the sidewall of the rotating cylinder, an active solution is injected in the rotating cylinder in an atomization mode, through the rotation of the rotating cylinder, under dipping by the active solution, and the catalyst carrier is capable of moving from a charging end at high position to a discharging end at low position of the rotating cylinder. According to the invention, the rotating cylinder capable of executing the dipping step in the preparation method is aslant arranged, so that the catalyst carrier is dipped by the active solution and simultaneously moves from the charging end to the discharging end, continuous preparation of the catalyst can be realized, and because that the material turning piece is arranged on the sidewall of the rotating cylinder, when the rotating cylinder is rotated, the catalyst carrier is capable of being turned over by the material turning piece, the catalyst carrier and the active solution are effectively contacted, and the dipping effect of the catalyst carrier is increased.

Description

technical field [0001] The invention relates to the field of preparation of catalysts, in particular to a preparation method of catalysts. Background technique [0002] In the catalyst preparation and production process, there are many production methods, such as impregnation method, roll coating method, precipitation method, mixing method, ion exchange method, gas phase synthesis method and so on. Among them, the impregnation method is a more commonly used method. In the impregnation method, the impregnation step of impregnating the active component in the active component solution onto the catalyst support is the most important step. [0003] In the prior art, the traditional equipment for realizing the above impregnation steps can refer to the impregnation tanks, impregnation baskets, impregnation mesh belts, impregnation drums, and impregnation drums recorded in "Catalyst Preparation Process Technology", Zhang Jiguang, P329-331. , Impregnation rolling machine, impregna...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J37/02B01J23/883B01J23/75B01J23/50B01J23/22B01J23/44
Inventor 侯朝鹏孙霞夏国富李明丰吴玉晋超阎振楠李猛胡志海聂红李大东
Owner CHINA PETROLEUM & CHEM CORP
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