A kind of release agent and preparation method thereof
A technology of release agent and additive, which is applied in the field of release agent and its preparation, and can solve the problems that the release agent is easy to fall off, etc.
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[0020] The present invention also provides a kind of preparation method of release agent, and this method comprises the following steps:
[0021] S1, mixing the additive with a surfactant to prepare an additive emulsion;
[0022] S2, mixing the silicone oil with an emulsifier to obtain a water-soluble release agent;
[0023] S3, mixing the additive emulsion with a water-soluble release agent to obtain a release agent;
[0024] Wherein, the additive is one or a mixture of nano-magnetic materials and nano-metal materials; based on the total weight of the release agent, the content of the additive is 1.6-24.5 wt%.
[0025] According to the preparation method of the release agent provided by the present invention, in order to make the release agent mix more uniformly, preferably, mechanical stirring and ultrasonic oscillation are carried out during the whole preparation process.
[0026] The mold release agent of the present invention, in the case of the overall magnetization of...
Embodiment 1
[0029] 1. Prepare nano-Fe powder by inert gas condensation method, the particle size is 30nm;
[0030] 2. Under the conditions of mechanical stirring and ultrasonic oscillation, prepare nano-iron powder emulsion, its composition and weight percentage are as follows: nano-Fe powder 90%wt, surfactant (PVA: Span 80 = 1:1): 10%wt ;
[0031] 3. Hydroxyl silicone oil and polyoxyethylene lauryl ether are mixed to form a water-soluble release agent, the content of hydroxyl silicone oil is 85wt%, and the content of polyoxyethylene lauryl ether is 15wt%;
[0032] 4. Under the condition of mechanical stirring and ultrasonic vibration, prepare magnetic release agent A1, its composition and weight percentage are as follows: 10%wt of nano-iron powder emulsion, 90%wt of water-soluble release agent.
Embodiment 2
[0034] 1. Preparation of nano-Fe by chemical precipitation method 3 o 4 Magnetic particles with a particle size of 60nm;
[0035] 2. Under the condition of mechanical stirring and ultrasonic vibration, prepare magnetic particle emulsion, its composition and weight percentage are as follows: magnetic particle 92%wt, surfactant (PVA): 8%wt;
[0036] 3. Hydroxy silicone oil and polyethylene glycol lauryl ether are mixed to form a water-soluble release agent, the content of hydroxyl silicone oil is 90wt%, and the content of polyethylene glycol lauryl ether is 10wt%;
[0037] 4. Under the condition of mechanical stirring and ultrasonic vibration, prepare magnetic release agent A2, its composition and weight percentage are as follows: magnetic particle emulsion 12%wt, water-soluble release agent 88%wt.
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