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A method for improving oil resistance of soybean protein isolate film

A soybean protein isolate and oil-blocking technology, which is applied in the field of polymer materials, can solve the problems of unfavorable amplification, reduced oil-blocking performance, and difficulty in adapting to industrial production.

Active Publication Date: 2017-02-22
CHANGSHU INSTITUTE OF TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Tang Yali and others studied the effect of using plasticizer and drying temperature on the oil resistance performance of soybean protein film, and found that increasing the amount of plasticizer can increase the elongation at break of the film and reduce the tensile strength of the film, but it has no effect on the oil resistance performance. The effect is not obvious
Heat treatment of the membrane liquid can increase its tensile strength and elongation at break, but it will increase the oil permeability coefficient and reduce the oil resistance performance
Although some methods can improve the oil resistance of soybean protein films to a certain extent, they are not conducive to scale-up, and it is difficult to meet the needs of industrial production.

Method used

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  • A method for improving oil resistance of soybean protein isolate film

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Soy protein isolate at a concentration of 50 mg / mL was dissolved in distilled water to form a suspension. Heat and stir in a water bath at 80 °C for 90 min, add 5% sucrose stearate ( W / W , sucrose stearate / protein), and stirred evenly at high speed to form a transparent solution, filtered, and degassed. The mixed solution was poured onto a plexiglass plate and cast evenly, and placed horizontally for 2 h. After the surface of the film was formed, it was dried in an oven at 80 °C for 2 h, and the film was immediately removed, and stored in a desiccator at a temperature of 25 °C and a relative humidity of 50% for 48 h before use.

[0023] According to the measurement method of the above-mentioned oil permeability coefficient, measure the oil permeability coefficient of the SPI membrane po is 3.45 g mm / (m 2 d).

Embodiment 2

[0025] Soy protein isolate at a concentration of 50 mg / mL was dissolved in distilled water to form a suspension. Heat and stir in a water bath at 50 °C for 150 min, add 15% sucrose palmitate ( W / W , sucrose palmitate / protein), and stirred at high speed to form a transparent solution, filtered, and degassed. The mixed solution was poured onto a plexiglass plate and cast evenly, and placed horizontally for 2 h. After the surface of the film was formed, it was dried in an oven at 80 °C for 2 h, and the film was immediately removed, and stored in a desiccator at a temperature of 25 °C and a relative humidity of 50% for 48 h before use.

[0026] According to the measurement method of the above-mentioned oil permeability coefficient, measure the oil permeability coefficient of the SPI membrane po is 5.71 g mm / (m 2 d).

Embodiment 3

[0028] Soy protein isolate at a concentration of 50 mg / mL was dissolved in distilled water to form a suspension. Heat and stir in a water bath at 65 °C for 30 min, add 25% sucrose oleate ( W / W , sucrose oleate / protein), and stirred evenly at high speed to form a transparent solution, filtered, and degassed. The mixed solution was poured onto a plexiglass plate and cast evenly, and placed horizontally for 2 h. After the surface of the film was formed, it was dried in an oven at 80 °C for 2 h, and the film was immediately removed, and stored in a desiccator at a temperature of 25 °C and a relative humidity of 50% for 48 h before use.

[0029] According to the measurement method of the above-mentioned oil permeability coefficient, measure the oil permeability coefficient of the SPI membrane po is 7.43 g mm / (m 2 d).

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Abstract

The invention relates to a method for improving oil resistance of an isolated soy protein film. The method is characterized by comprising the steps of dissolving isolated soy protein in distilled water to form suspension, heating and stirring in a water bath at a certain temperature, adding fatty acid sucrose ester, stirring uniformly at a high speed to form a clear solution, carrying out filtration and degassing, pouring the mixed solution onto an organic glass plate for uniform flow casting, placing horizontally, and putting in an oven for drying and film forming after forming of the surface of the film. The method can greatly improve the oil resistance of the isolated soy protein film, retard oil migration and diffusion and ensure stable product quality.

Description

technical field [0001] The invention belongs to the field of macromolecular materials, and in particular relates to a method for improving the oil resistance performance of a soybean protein isolate film. Background technique [0002] Edible food packaging film is a new type of porous network structure film made of natural edible substances. After realizing the packaging function, it can be transformed into a kind of edible raw material. The packaging material will not produce waste and can maximize the use of resources. Therefore, it will be one of the key points in the development of the packaging industry in the future. Among the existing edible packaging films, the development of edible soy protein isolate (SPI) film is favored by packaging material researchers. Due to the excellent film-forming properties, oxygen barrier properties and high nutritional value of soybean protein isolate, it has attracted much attention in the development of edible films. [0003] The o...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08J5/18C08L89/00C08K5/103
Inventor 王立梅齐斌朱益波朱颖越梁剑光郑丽雪
Owner CHANGSHU INSTITUTE OF TECHNOLOGY