A kind of filter spice stick of graphene-polymer composite airgel and preparation method thereof
A composite aerogel and graphene technology, applied in food science, e-liquid filter, application, etc., can solve the problems of loss of harm reduction and aroma enhancement, and achieve the effects of good market application prospects, simple operation and novel appearance.
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Embodiment 1
[0026] Add 1 g of acrylic acid, 0.05 g of sodium persulfate, 0.001 g of N,N'-methylenebisacrylamide, and 0.005 g of graphene oxide to 10 g of water, stir well, ultrasonically treat it at 20°C for 20 min, add a circular In the mold, pass nitrogen protection, heat to 50 ° C, react for 6 hours, take out, add water to wash and swell balance for 48 hours, and then freeze-dry at -50 ° C for 1 hour; after taking out, spray with the tobacco flavor material to obtain graphite. Ethene-polymer composite aerogel filter fragrance stick. The obtained round flavor stick is added to the filter tip to prepare a cigarette, the tar content of the smoke is reduced, the cool feeling is enhanced, and the comfort and the elegant feeling of the smoke are enhanced.
Embodiment 2
[0028] Add 1 g of acrylamide, 0.005 g of ammonium persulfate, 0.01 g of N,N'-methylenebisacrylamide, and 0.005 g of graphene oxide into 50 g of water, stir evenly, ultrasonically treat it at 20°C for 20 minutes, and add it to a triangular mold In the medium, nitrogen protection, heated to 70 ℃, the reaction time is 0.5 hours, take out, add methanol cleaning agent to clean and swell for 12 hours, and then freeze-dry at -10 ℃ for 6 hours; That is, the graphene-polymer composite aerogel filter fragrance stick is obtained. The obtained triangular spice stick is added to the filter tip to prepare a cigarette, the tar content of the smoke is reduced, the aroma volume is increased, and the comfort and elegant feeling of the smoke are enhanced.
Embodiment 3
[0030] Add 0.5 g of acrylamide, 0.5 g of acrylic acid, 0.025 g of potassium persulfate, 0.015 g of N,N'-methylenebisacrylamide, and 0.015 g of graphene oxide to 20 g of water, stir well, and ultrasonically treat at 20°C 20min, put it into the pentagonal mold, pass nitrogen protection, heat to 60 °C, the reaction time is 5 hours, take it out, add acetone cleaning agent to clean and swell for 30 hours, and then supercritically dry with carbon dioxide, the supercritical condition is 30 °C, 7 MPa , dried for 48 hours, taken out and sprayed with fragrance substances extracted from plants such as flowers and plants to obtain a graphene-polymer composite aerogel filter tip fragrance stick. The obtained pentagonal flavor stick is added to the filter tip to prepare a cigarette, the tar amount of the smoke is reduced, the aroma amount is increased, the cool feeling is enhanced, and the smoke comfort and elegant feeling are enhanced.
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