Unlock instant, AI-driven research and patent intelligence for your innovation.

Degreasing method for low-ester pectin

A low-ester pectin and de-esterification technology, applied in fermentation and other directions, can solve the problems of inability to extract pectin, low pectin content, reduced pectin gelation degree and esterification degree, etc., so as to break the technological monopoly and reduce production. cost, the effect of improving production efficiency

Inactive Publication Date: 2015-10-14
安徽亿源生物工程有限公司
View PDF2 Cites 5 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] (1) Acid method deesterification: The obtained pectin polygalacturonic acid content is relatively high, but the reaction speed is slow. Under the same temperature and concentration conditions, its deesterification speed is much lower than that of alkaline method deesterification, and the temperature rise can be accelerated reaction speed, but the depolymerization speed of pectin chains will also be greatly accelerated, seriously destroying the gel strength of pectin
[0004] (2) Alkaline deesterification: its deesterification speed is fast, but when pectin is deesterified by alkaline method, in addition to the reduction of methoxyl content in the molecule, it will also produce depolymerization of pectin molecules, that is, β-elimination reaction , leading to a decrease in pectin molecular weight, viscosity, and gelation degree
[0005] (3) Enzymatic deesterification: In the process of pectin extraction, add pectinase for direct deesterification; Disadvantages: First, due to the long time of pectin extraction, pectinase has destroyed a large number of pectin molecular chains, reducing the The degree of gelation and esterification of pectin seriously affects the quality of pectin; secondly, the quality requirements for raw materials for pectin production are relatively high, and raw materials with low gum content will be depleted due to the long-term action of pectinase during the extraction process. As a result, a large amount of pectin is destroyed, and pectin cannot be extracted in the end; third, a higher temperature is required during the extraction process, which seriously destroys the activity of pectinase, so that a large amount of pectinase does not play a corresponding role, resulting in pectin Too much glue enzyme

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] Embodiment 1: a kind of deesterification method of low-ester pectin, comprises the following steps:

[0018] (1) Crush one or more of fresh orange peels, watermelon peels, apple peels, sunflower discs and rods to a particle size of 2mm, mix the obtained raw materials with water eight times its weight, heat to 90°C, and add carbonic acid Adjust the pH of the solution to 7 with sodium and keep it warm for 2 hours;

[0019] (2) Filter the above solution, wash the obtained filter residue repeatedly with warm water at 50°C until it is colorless and odorless, add hydrochloric acid, adjust the pH to 1.5, extract at 60°C for 30 minutes, and filter with suction to obtain the filtrate;

[0020] (3) Concentrate the filtrate in vacuum to obtain a concentrated solution of high-ester pectin, add ammonia water to the concentrated solution to adjust the pH to 3.5, cool to 25°C and add pectinase at 0.0125% of the concentrated solution to perform a deesterification reaction, After 2 hou...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a degreasing method for low-ester pectin. According to the degreasing method, pectinase directly acts on a high-ester pectin concentrated solution, so that dosage of pectinase is reduced greatly; by controlling temperature of the concentrated solution, the activity of pectinase is kept, and pectinase plays the role of degreasing; and after degreasing, precipitation is carried out quickly, so that production efficiency is improved greatly, and the production cost is reduced. The degreasing method has the advantages of high extraction efficiency, high production efficiency, high product quality and simple process, and is very suitable for scale production and industrial production. The low-ester pectin production process provided by the invention not only fills the blank of industrially producing low-ester pectin inland, but also breaks the monopoly of foreign manufacturers on low-ester pectin products, industrial development of low-ester pectin in our country is facilitated, and a national pectin brand is built.

Description

technical field [0001] The invention relates to pectin, in particular to a method for deesterifying low-ester pectin. Background technique [0002] At present, the deesterification process of pectin includes: acid deesterification, alkaline deesterification and enzymatic deesterification. [0003] (1) Acid method deesterification: The obtained pectin polygalacturonic acid content is relatively high, but the reaction speed is slow. Under the same temperature and concentration conditions, its deesterification speed is much lower than that of alkaline method deesterification, and the temperature rise can be accelerated The reaction speed, but the depolymerization speed of the pectin chain will be greatly accelerated, seriously destroying the gel strength of pectin. [0004] (2) Alkaline deesterification: its deesterification speed is fast, but when pectin is deesterified by alkaline method, in addition to the reduction of methoxyl content in the molecule, it will also produce ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C12P19/14C12P19/04
Inventor 李恒勇李大伟郭芳何利影周光姣夏成凯
Owner 安徽亿源生物工程有限公司