OLED alloy cathode and preparation method thereof
A kind of alloy and cathode technology, which is applied in semiconductor/solid-state device manufacturing, electrical components, electric solid-state devices, etc., can solve the problems of unbalanced device positive load carrier injection, weak ability of cathode to emit electrons, easy oxidation or peeling, etc. Achieve the effects of reducing the difficulty of preparation, easy control of film thickness, and reducing the difficulty of operation
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[0023] A preparation method of OLED alloy cathode, comprising the following steps:
[0024] Step 1, Ca, Mg, Al raw material preparation: adopt the electronic balance of 1 / 10,000 to weigh Ca respectively according to the mass ratio Ca:Mg:Al=15%: (5%-25%): (80%-60%) , Mg, Al raw materials;
[0025] Step 2, preparation of the quartz glass tube: cut off the required length of the quartz glass tube, and use a mixed gas of oxygen and liquefied petroleum gas to melt and seal one end of the quartz glass tube for use;
[0026] Step 3, sealing of raw materials: Put the weighed Ca, Mg and Al raw materials into a quartz glass tube with one end closed, vacuumize the quartz glass tube and burn the other end of the quartz glass tube with a mixed gas of oxygen and liquefied petroleum gas melting seal;
[0027] Step 4, preparation of the alloy cathode: Put the sealed quartz glass tube with raw materials into the high-temperature sintering furnace. The temperature setting of the high-temperat...
Embodiment 1
[0029] This embodiment is an OLED alloy cathode, including 20% Mg, 15% Ca, and 65% Al. Among them, the work function of Al is 4.28ev, the work function of Mg is 3.7ev, and the work function of Ca is 2.87ev. It is formed by melting in a quartz glass tube under vacuum conditions by vacuum melting and then cooling naturally.
[0030] The preparation process is as follows:
[0031] Step 1, preparation of Ca, Mg and Al raw materials: Use an electronic balance of 1 / 10,000 to separate the required Al wire, Ca particles, and Mg particles according to the mass ratio of Ca:Mg:Al=15%:20%:65%. Appreciate;
[0032] Step 2, preparation of the quartz glass tube: cut off the required length of the quartz glass tube, and burn and seal one end of the quartz glass tube with a mixed gas of oxygen and liquefied petroleum gas for use;
[0033] Step 3, sealing of raw materials: Put the weighed Ca, Mg and Al raw materials into a quartz glass tube with one end closed, vacuumize the quartz glass t...
Embodiment 2
[0036] This embodiment is an OLED alloy cathode, including 5% Mg, 15% Ca, and 80% Al. Among them, the work function of Al is 4.28ev, the work function of Mg is 3.7ev, and the work function of Ca is 2.87ev. It is formed by melting in a quartz glass tube under vacuum conditions by vacuum melting and then cooling naturally.
[0037] The preparation process is as follows:
[0038] Step 1, preparation of Ca, Mg and Al raw materials: Use an electronic balance of 1 / 10,000 to separate the required Al wire, Ca particles, and Mg particles according to the mass ratio of Ca:Mg:Al=15%:5%:80%. Appreciate;
[0039] Step 2, preparation of the quartz glass tube: cut off the required length of the quartz glass tube, and burn and seal one end of the quartz glass tube with a mixed gas of oxygen and liquefied petroleum gas for use;
[0040] Step 3, sealing of raw materials: Put the weighed Ca, Mg and Al raw materials into a quartz glass tube with one end closed, vacuumize the quartz glass tube ...
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