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Process for producing wear-resistant highly-elastic butyl chloride regenerated rubber

A chlorinated butyl rubber and chlorinated butyl technology, applied in the direction of plastic recycling, recycling technology, etc., can solve the problems of general wear resistance, unsatisfactory, poor elastic properties, etc., and achieve the improvement of elasticity and wear resistance. Effect

Inactive Publication Date: 2015-11-11
NANTONG DEAN CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, only antioxidants, softeners and plasticizers are added in the traditional production process of chlorobutyl reclaimed rubber. Although the production process is less, the products produced have general wear resistance and poor elasticity, and the desulfurization process is The required heat energy is generally provided by electric heating, which consumes a lot of energy and cannot meet the requirements of modern industry, especially in the field of tires that have high requirements for elasticity and wear resistance.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A process for producing wear-resistant and highly elastic chlorinated butyl regenerated rubber, comprising the following steps:

[0023] a: waste chlorobutyl rubber raw material is inspected, cleaned and removed;

[0024] b: Put the raw materials into the pulverizer for pulverization and granulation to form 2-purpose colloidal particles;

[0025] c: put 80 parts by weight of colloidal particles, 0.2 parts by weight of p-phenylenediamine and 0.8 parts by weight of rosin into a desulfurization device for desulfurization. The desulfurization temperature is 200°C, the desulfurization pressure is 3.8Mpa, and the desulfurization time is 1h. The heat energy required in the desulfurization process is the heat energy converted from solar energy;

[0026] D: add the copolymer of styrene and butadiene of 0.6 weight part, the promotor D of 0.3 weight part, the fatty acid amide of 0.1 weight part and the aluminum hydroxide of 0.2 weight part to process again;

[0027] e: Cooling, ...

Embodiment 2

[0029] A process for producing wear-resistant and highly elastic chlorinated butyl regenerated rubber, comprising the following steps:

[0030] a: waste chlorobutyl rubber raw material is inspected, cleaned and removed;

[0031] b: Put the raw materials into the pulverizer for pulverization and granulation to form 3-purpose colloidal particles;

[0032] c: Put 90 parts by weight of colloidal particles, 0.3 parts by weight of p-phenylenediamine and 0.9 parts by weight of rosin into a desulfurization device for desulfurization. The desulfurization temperature is 210°C, the desulfurization pressure is 3.9Mpa, and the desulfurization time is 1.25h , the heat energy required in the desulfurization process is the heat energy converted from solar energy;

[0033] D: add the copolymer of 0.7 weight part styrene and butadiene, the accelerator D of 0.4 weight part, the fatty acid amide of 0.2 weight part and the aluminum hydroxide of 0.3 weight part to process;

[0034] e: Cooling, te...

Embodiment 3

[0036] A process for producing wear-resistant and highly elastic chlorinated butyl regenerated rubber, comprising the following steps:

[0037] a: waste chlorobutyl rubber raw material is inspected, cleaned and removed;

[0038] b: Put the raw materials into the pulverizer for pulverization and granulation to form 4-purpose colloidal particles;

[0039] c: Put 100 parts by weight of colloidal particles, 0.4 parts by weight of p-phenylenediamine and 1 part by weight of rosin into a desulfurization device for desulfurization. The desulfurization temperature is 220°C, the desulfurization pressure is 4.0Mpa, and the desulfurization time is 1.5h , the heat energy required in the desulfurization process is the heat energy converted from solar energy;

[0040] D: add the copolymer of styrene and butadiene of 0.8 weight part, the promotor D of 0.5 weight part, the fatty acid amide of 0.3 weight part and the aluminum hydroxide of 0.4 weight part to process again;

[0041] e: Cooling,...

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PUM

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Abstract

The invention provides a process for producing wear-resistant highly-elastic butyl chloride regenerated rubber. The process comprises the following steps: a, conducting testing, cleaning and impurity removing on a waste butyl chloride rubber raw material; b, feeding the raw material into a pulverizer to be pulverized and granulated to form colloidal particles; c, feeding the colloidal particles, an antioxygen and a plasticizing agent into a desulfurizing device for desulfurization; d, adding a toughening agent, an accelerating agent, a lubricating agent and a fire retarding agent for processing; e, cooling, detecting and packaging a processed product. The process has the benefits that a series of additives of the toughening agent, the accelerating agent, the lubricating agent and the like is added for processing, the elasticity and the abrasion resistance of the product is effectively improved, moreover, heat energy needed in the production process is converted from solar energy, and energy conservation and environmental protection are achieved.

Description

technical field [0001] The invention relates to a production process of rubber materials, in particular to a process for producing wear-resistant and highly elastic chlorinated butyl regenerated rubber. Background technique [0002] Chlorobutyl rubber has all the inherent characteristics of butyl rubber, but also has a series of advantages such as fast vulcanization speed, co-vulcanization with other rubbers, more heat resistance, and small compression deformation. Therefore, it is widely used in tires, industrial rubber products, building sealing materials and other fields. However, only antioxidants, softeners and plasticizers are added in the traditional production process of chlorobutyl reclaimed rubber. Although the production process is less, the products produced have general wear resistance and poor elasticity, and the desulfurization process is The required heat energy is generally provided by electric heating, which consumes a lot of energy and cannot meet the req...

Claims

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Application Information

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IPC IPC(8): C08J11/10C08L17/00C08L23/28C08L25/10C08K5/20C08K3/22
CPCY02W30/62
Inventor 张忍
Owner NANTONG DEAN CHEM
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