Fullerene, boron and nitrogen containing lubricant and preparation method thereof
A fullerene boron nitrogen lubricant, fullerene technology, applied in lubricating compositions, additives, petroleum industry and other directions, can solve problems such as use restrictions, and achieve good lubricity and significant fuel-saving effects.
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[0016] The preparation method of the fullerene boron nitrogen lubricant of the present invention is based on the reaction of fullerene C60 with concentrated sulfuric acid and concentrated hydrochloric acid, then adding tall oil acid, and adopting the method of adjusting the pH value to obtain polar modified fullerene , then react with methyl laurate, nitrogen-containing borate, take two-step partial pressure decompression method, obtain fullerene boron nitrogen lubricant, comprising the following steps:
[0017] 1) Synthesis of polar modified fullerenes
[0018] Put fullerene C60, concentrated sulfuric acid, and concentrated hydrochloric acid in a container, and react under vacuum at 90°C to 100°C for 2 to 3 hours, then ultrasonically wash with water and amine, adjust the pH to 7, add tall oleic acid, Continue to react at a temperature of 200-220°C for 3-4 hours, then vacuum filter to obtain a precipitate, wash with alcohol and ultrasonic water to neutrality, and obtain a brow...
Embodiment 1
[0034] 1. Synthesis of polar modified fullerenes
[0035] Put fullerene C60, concentrated sulfuric acid, and concentrated hydrochloric acid in a container, and react at 100°C under vacuum (pressure = 0.095MPa) for 2 hours, then ultrasonically wash with water and amine, adjust the pH to 7, and add tall oleic acid. Continue to react at a temperature of 200°C for 3 hours, then vacuum filter to obtain a paste mixture, wash with alcohol and ultrasonic water until neutral, and obtain a brown paste which is polar-modified fullerene;
[0036] Fullerene C60: Concentrated sulfuric acid: Concentrated hydrochloric acid: Tall oil = 1:5:5:22 (weight ratio).
[0037] 2. Synthesis of fullerene boron nitrogen lubricant
[0038] Mix 5 grams of the polar-modified fullerene prepared above with 10 grams of methyl laurate, stir evenly, and react for 4 hours at a temperature of 100°C and a pressure of 0.1MPa; cool to 40°C, and add nitrogen-containing borate 100 grams, increase the temperature to 2...
Embodiment 2
[0041] 1. Synthesis of polar modified fullerenes
[0042] Put fullerene C60, concentrated sulfuric acid and concentrated hydrochloric acid in a container, react at 90°C under vacuum (pressure = 0.095MPa) for 3 hours, then wash with ultrasonic water and amine, adjust the pH to 7, and add tall oleic acid , continue to react at a temperature of 220° C. for 4 hours, then vacuum filter to obtain a paste mixture, wash with alcohol and ultrasonic water to neutrality, and obtain a brown paste which is polar modified fullerene;
[0043] Fullerene C60: Concentrated sulfuric acid: Concentrated hydrochloric acid: Tall oil = 1:7:7:25 (weight ratio).
[0044] 2. Synthesis of fullerene boron nitrogen lubricant
[0045]Mix 10 grams of the polar-modified fullerene prepared above with 15 grams of methyl laurate, stir evenly, and react for 5 hours at a temperature of 120°C and a pressure of 0.1MPa; cool to 50°C, and add nitrogen-containing borate 250 grams, increase the temperature to 210°C, c...
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