Method for measuring ammonia content in mainstream smoke of cigarettes
A technology for cigarette mainstream smoke and mainstream smoke, which is applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of cumbersome processing steps and heavy workload, and achieve simplified ammonia capture devices and steps, simple operation, and efficient capture Set device for simple effects
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[0048] 1) Reagents and instruments used
[0049] Reagents: hydrochloric acid, methanesulfonic acid, Kentucky 3R4F reference sample, ultrapure water, 1000mg / LNH 4 + Standard solution, ultrapure water;
[0050] Instruments: ion chromatograph (equipped with column thermostat, gradient pump, cation suppressor and conductivity detector), SM450 smoking machine, balance, ultrasonic generator, pure water meter, 0.45μm aqueous phase filter membrane, 5mL disposable syringe, Φ44mm Cambridge filter (whatmanF319-04).
[0051] Cigarette sample preparation: the Kentucky 3R4F cigarette sample was placed in an environment with a temperature of 22°C±1°C and a relative humidity of 60%±2% for 48 hours.
[0052] 2) Preparation of filter disks: According to the volume of hydrochloric acid shown in Table 1, the concentration of hydrochloric acid and the time placed in the fume hood, the Cambridge filter disks containing hydrochloric acid in Examples 1-3 were prepared respectively. Specifically, ...
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