An anti-angiogenic polypeptide [d-ala1]as16
An anti-angiogenesis, AS16 technology, applied in the field of polypeptide [D-Ala1] AS16, can solve the problems of treatment effect, easy to be degraded by enzymes, short half-life, etc., and achieve the goal of delaying animal weight growth, not easy to be degraded by enzymes, and long half-life Effect
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Embodiment 1
[0052] The anti-angiogenic polypeptide provided by the application [D-Ala 1 ]AS16, containing 16 amino acids, with a molecular weight of 1683.0, the specific amino acid sequence is:
[0053] D-Ala-Thr-Trp-Leu-Pro-Pro-Arg-Ala-Ala-Asn-Leu-Leu-Met-Ala-Ala-Ser; ie
[0054] D-ATWLPPRAANLLMAAS;
[0055] Wherein said D-Ala and D-A represent that the first amino acid alanine in the polypeptide sequence is in D-configuration.
[0056] Polypeptide [D-Ala 1 ]AS16 is prepared by Fomc solid-phase peptide synthesis method, the specific preparation process is as follows:
[0057] (1) To swell the resin, weigh 0.3g of Wang resin, then pour the weighed Wang resin into the cleaned and dried peptide synthesizer, then add 5 mL of DMF, and swell the resin for 30 minutes. After swelling, use a vacuum pump Extract the DMF from the peptide synthesizer;
[0058] (2) the addition of the first amino acid,
[0059] Calculate and weigh 316.5 mg of serine, 111.5 mg of HOBT (1-hydroxybenzotriazole) an...
Embodiment 2
[0097] This example mainly introduces the relevant drug experiments using the Balb / c mouse transplanted tumor model (loaded with H22 mouse liver cancer cells) as the biological material, including the tumor inhibition rate experiment, tail vein injection experiment, mouse survival experiment, etc. Multiple, so that a more comprehensive response to the polypeptide [D-Ala 1] The effect of AS16 on anti-tumor angiogenesis. The details of relevant experiments are introduced as follows.
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