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1139results about How to "Not easy to degrade" patented technology

Water-collecting polymer filament imitating spider silk structure and preparation method thereof

ActiveCN102776785AHigh affinityHigh fog water collection efficiencyFibre treatmentSpider ProteinsPolymer science
The invention relates to water-collecting polymer filament imitating the spider silk structure and a preparation method thereof. The preparation method comprises the following steps of: immersing common artificial silks into polymer solution mixed by a good solvent and a poor solvent containing polymer, then horizontally pulling out the artificial silks from the polymer solution along the axial direction of the artificial silks, and further enabling the polymer solution to wrap the surfaces of the artificial silks to form a liquid film; then due to Rayleigh instability, causing that the liquid film of the polymer solution on the surfaces of the artificial silks evolutes (break) into a string of liquid drops hung on the artificial silks; by adjusting the humidity and the temperature of the environment, drying the polymer liquid drops hung on the artificial silks so as to form spindle knots with periodic arrangement and a spindle-shaped structure on the surfaces of the artificial silks; and enabling the spindle knots which are in alignment along the axial direction of the artificial silks to form a coarse structure on the surfaces of the artificial silks, and further obtaining the water collecting polymer silks with the similar spider-silk structure by biomimetic synthesis.
Owner:INST OF CHEM CHINESE ACAD OF SCI

Preparation method and application of hydrophobic modified guar gum

InactiveCN102827300ANot easy to degradePreserve macromolecular quality propertiesWater-repelling agents additionCelluloseOrganic acid
The invention discloses a preparation method and an application of hydrophobic modified guar gum. The method comprises the following steps of: suspending guar gum in an ionic liquid, adding a basic catalyst, and alkalifying at the temperature of 10-40 DEG C; gradually heating under the protection of nitrogen, dropwise adding a modifying agent slowly, and heating to 30-80 DEG C for performing a modification reaction; and after the reaction, adding organic acid for adjusting the pH to 5-7, soaking and washing with ethanol, filtering, and drying a filter cake in vacuum to obtain the hydrophobic modified guar gum. A hydrophobic alkyl long chain is introduced into guar gum hydroxyl, and a terminal group is a carboxylic acid group, so that the water dissolving speed of the guar gum is increased, the macromolecular quality characteristic of the guar gum is protected to the maximum extent, and the guar gum is endowed with hydrophobic performance. Compared with other modified guar gum, the hydrophobic guar gum has the advantages of high molecular weight, high compatibility with cellulose, increase in the molecular bonding force of cellulose-guar gum, improvement on the paper strength and applicability to a paper-making wet part chemical process as a reinforcing agent and a surface sizing agent.
Owner:SOUTH CHINA UNIV OF TECH

Microcapsule insecticide-fertilizer preparation, preparation method and application thereof

The invention discloses a microcapsule insecticide-fertilizer preparation, a preparation method and application thereof. The preparation consists of the following components in part by weight: 1 to 30 parts of pesticide microcapsules and 70 to 99 parts of nutrient substance. The preparation method mainly comprises the following steps of: after fully dissolving a pesticide with a solvent, adding a wall material monomer into solution and mixing uniformly; transporting a mixture into a shear dispersion reaction kettle which is filled with smashed capsule bodies; stirring the mixture and the capsule bodies so that the capsules fully absorb the solution; performing a shear dispersion reaction to form capsules; performing solid-liquid separation and drying to prepare the pesticide microcapsules; adding the nutrient substances into the pesticide microcapsules; and fully stirring and uniformly mixing to prepare the microcapsule insecticide-fertilizer preparation. By using the microcapsule insecticide-fertilizer preparation and the preparation method, the problems of the chemical compatibility and the physical stability of the conventional insecticide-fertilizer preparation in the same system are solved effectively. A product of the invention has the advantages of: shielding and slow-releasing functions, high chemical compatibility and physical stability, lasting pesticide effect, natural degradability, no environment pollution, low use cost and simple production process.
Owner:侯金荣 +1

Preparation method of freshwater collecting fibers with transmission function and application thereof

The invention discloses a preparation method of freshwater collecting fibers with a transmission function and an application thereof and belongs to the technical field of chemical bionics. The preparation method comprises the following steps of: completely soaking a support fixed with the fibers in a prepared polymer solution with the mass fraction of 5-9% for lifting and pulling, wherein raised nodes, which are sequentially arrayed according to the size, are generated on the fibers, and finally drying to obtain the freshwater collecting fibers. The freshwater collecting fibers are woven intothe freshwater collecting fiber net for carrying out freshwater collection; and the freshwater collecting fiber net can be used for collecting freshwater in fog so that the visibility of air can be increased; and the freshwater collecting fiber net has high water collection efficiency and can be used for removing fog. The heights of the raised nodes on the surfaces of the fibers prepared by the method are uniformly increased from small to large and are controlled; the surfaces of the fibers are provided with more microscopic bulges or micropores so that the collision probability and the spreading speed of water drops in air can be increased, and the efficiency of collecting water is increased; and the freshwater collecting fibers are suitable for coastal deserts, islands, ocean ships, foggy mountain areas and the like; and the cost of the freshwater collecting fiber for collecting the freshwater is far lower than the cost for the desalination of sea water.
Owner:BEIHANG UNIV

Surface modifying method for improving surface power function of indium tin oxide transparent conductive film

InactiveCN102610765AHigh surface work functionDoes not degrade surface finishSolid-state devicesSemiconductor/solid-state device manufacturingHigh energyOxygen ions
The invention belongs to the technical filed of conductive thin films, in particular relates to a surface modifying method for improving the surface power function of an indium tin oxide transparent conductive film. The surface modifying method comprises the following steps: a large volume of plasma, containing oxygen, chlorine, or fluorine strong electric negative elements, is generated in a vacuum chamber in a radio frequency or microwave discharge excitation way; sheet glass coated with an indium tin oxide (ITO) thin film is placed on a metal substrate bench which is dipped in the plasma; high voltage negative pulses are applied on the substrate bench, thus forming a negative voltage sheath layer between the ITO thin film and the plasma; oxygen ions are accelerated by an electric field to move toward the surface of the ITO thin film in the sheath layer; and high-energy oxygen ions are injected to the surface of the ITO thin film and reserved in a surface layer of the ITO thin film, so that O / (Sn+In) atom proportion of the surface of the ITO thin film is increased, and then the surface power function of the ITO thin film is improved. The ITO thin film modified by the surface modifying method provided by the invention is applied as an anode of an organic light emitting diode (OLED), in this way, the drive voltage of a component is reduced greatly, the current stability of the component is improved, the light efficiency and brightness are enhanced, and the service life of the component is prolonged.
Owner:FUDAN UNIV

Oxiracetam freeze-drying preparation for injection and preparation method thereof

The invention relates to an oxiracetam freeze-drying preparation for injection and a preparation method thereof, belonging to the technical field of medicines. The freeze-drying preparation is a crystal form compound formed by oxiracetam, D-sorbitol and mannitol in a weight ratio of 1: (0.2-0.25): (0.05-0.1). The oxiracetam freeze-drying preparation has the beneficial effects that the production cycle is shortened by about 20 hours, the rate of finished products is increased by above 99%, the phenomena such as the upward shifting and the eruption of the product are avoided, medicine molecules are constrained in crystal lattices, the water content is extremely low and can be controlled below 0.1%, the preparation is difficult to degrade and has relatively good stability, the period of validity is up to 36 months, the impurity content is greatly reduced, the single maximum impurity is less than 0.1%, and the total impurities are less than 0.5%; no organic solvents are involved in the production process, the energy consumption and the cost are substantially reduced, and the technology has environmentally-friendly effect and is suitable for large-scale industrialization production. Compared with the prior art, the oxiracetam freeze-drying preparation provided by the invention has obviously improved curative effect and is suitable for clinical application.
Owner:CSPC OUYI PHARM CO LTD

Human umbilical cord mesenchymal stem cell extract freeze-dried powder and preparation method

The invention relates to human umbilical cord mesenchymal stem cell extract freeze-dried powder and a preparation method. The preparation method of the human umbilical cord mesenchymal stem cell extract freeze-dried powder comprises the following steps: obtaining human umbilical cord mesenchymal primary stem cells, which are relatively high in purity, by virtue of density gradient centrifugation, conducting subculture, collecting a culture supernatant of the 3rd-18th generations of cells, and mixing the supernatant with trehalose, so that the freeze-dried powder is prepared. The human umbilical cord mesenchymal stem cell extract freeze-dried powder prepared by the invention has good appearance characteristics; the freeze-dried powder, when redissolved, is relatively rapid to dissolve and is completely dissolved; and animal experiments prove that the freeze-dried powder is low in irritation, high in safety and reliable to use. In addition, the freeze-dried powder disclosed by the invention can effectively preserve various bioactive cell factors in the human umbilical cord mesenchymal stem cell culture supernatant, protect skin from ultraviolet damage and promote the synthesis of skin collagen, and the freeze-dried powder has functions of whitening the skin and delaying aging.
Owner:广东省华桑丽皙生物技术有限公司

Adsorbent gel ball and preparation method thereof

The invention provides a preparation method for an absorptive gel ball. The method provided by the invention comprises the following steps: a) carrying out carboxylation processing on a carbon nano tube by utilizing the mixed solution of concentrated sulfuric acid and concentrated nitric acid to obtain a carboxyl modified carbon nano tube, wherein the weight ratio of the concentrated sulfuric acid to the concentrated nitric acid to the carbon nano tube is (40-90): (30-5): (30-5); b) mixing the carboxyl modified carbon nano tube and water soluble alginate in water to obtain the mixture of the alginate and the carbon nano tube; and c) adding a calcium chloride solution to the mixture to obtain the absorptive gel ball. The invention also provides an absorptive gel ball. The absorptive gel ball provided by the invention comprises multiple micro-gel balls in a core shell structure, wherein the core of the micro-gel ball is the carboxyl modified carbon nano tube; and the shell is a calcium alginate polymer. The absorptive gel ball provided by the invention has high absorption efficiency and is suitable for the processing of decoloration of wastewater in the fields such as textile, printing and dyeing, printing ink, leather, rubber, coking, papermaking, pharmacy and the like.
Owner:HUBEI UNIV

Preparation process of blueberry concentrated juice with high content of anthocyanin

The invention provides a preparation process of blueberry concentrated juice with high content of anthocyanin. According to the preparation process provided by the invention, pectase is adopted for performing enzymolysis on blueberry pulp, chitosan is adopted as a clarifying agent for obtaining clear blueberry juice, a decompression concentration process is adopted for preparing the blueberry concentrated juice, and microwave sterilization is adopted for sterilizing the blueberry concentrated juice. The preparation process comprises the following steps of: selecting blueberry fruits in vaccinium ashei gardenblue species; extracting the blueberry juice, and adding the pectase to perform the enzymolysis on the blueberry pulp; clarifying the blueberry juice, and adding the chitosan as the clarifying agent for obtaining the clear blueberry juice; concentrating the blueberry juice, and adopting the decompression concentration to obtain the blueberry concentrated juice; and performing sterile filling on the blueberry juice, and adopting the microwave sterilization to sterilize the blueberry concentrated juice, wherein the content of soluble solids in the blueberry concentrated juice is 60%-75%, and the content of the anthocyanin is 1.925g/L-3.384g/L. The preparation process provided by the invention can not only effectively prevent the loss of the anthocyanin in the blueberry concentrated juice, but also shorten the concentration time, control the production cost of the preparation process and effectively protect color, luster, fragrance and other sensory qualities of the blueberry juice.
Owner:ANHUI AGRICULTURAL UNIVERSITY
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