Preparation method for tellurium bismuth nano-crystalline solar cell panel
A technology of solar panels and nanocrystals, which is applied in the manufacture of electrolytic capacitors and photosensitive equipment, etc., can solve the problems of complex preparation process, lower output power of solar panels, low stability, etc. The effect of broad application prospects
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example 1
[0019] Admit argon gas into the glove box for protection, the ventilation rate is 10mL / min, until the air in the box is exhausted, add bismuth powder and tellurium powder into the planetary high-energy ball mill at a mass ratio of 2:3, according to the ball-to-material ratio Add tungsten carbide grinding balls for 10:1, set the speed of the main disc of the mill to 300r / min, and the reverse speed of the small disc to 500r / min, and mill for 12 hours, wherein the ball milling is continued after 30 minutes after one hour of ball milling to obtain a mixture of tellurium and bismuth. Powder; take 50g of the above-mentioned mixed tellurium-bismuth powder and put it into a three-necked flask with a stirrer, dropping funnel and thermometer, add 400mL polyethylene glycol dropwise through the dropping funnel, start the stirrer at a speed of 300r / min After stirring at a rotating speed for 20 minutes, move it into an ultrasonic disperser, ultrasonically disperse with a power of 200W for 1 ...
example 2
[0022]Pass argon gas into the glove box for protection, the ventilation rate is 13mL / min, until the air in the box is exhausted, add bismuth powder and tellurium powder into the planetary high-energy ball mill at a mass ratio of 2:3, Add tungsten carbide grinding balls to the ratio of 10:1, set the speed of the main disc of the mill to 350r / min, and the reverse speed of the small disc to 600r / min, and mill for 14 hours. After one hour of ball milling, continue ball milling after an interval of 30 minutes to obtain a mixture of tellurium and bismuth. Powder: Take 80g of the above-mentioned mixed tellurium-bismuth powder and put it into a three-necked flask with a stirrer, dropping funnel and thermometer, add 450mL polyethylene glycol dropwise through the dropping funnel, start the stirrer at a speed of 350r / min After stirring for 25 minutes at a rotating speed, move it into an ultrasonic disperser, ultrasonically disperse with a power of 250W for 1 hour, and then concentrate it ...
example 3
[0025] Pass argon gas into the glove box for protection, the ventilation rate is 15mL / min, until the air in the box is exhausted, add bismuth powder and tellurium powder into the planetary high-energy ball mill at a mass ratio of 2:3, Add tungsten carbide grinding balls at a ratio of 10:1, set the speed of the main disc of the mill to 400r / min, and the reverse speed of the small disc to 700r / min, and mill for 15 hours. After one hour of ball milling, continue ball milling after an interval of 30 minutes to obtain a mixture of tellurium and bismuth. Powder; take 100g of the above-mentioned mixed tellurium-bismuth powder and put it into a three-necked flask with a stirrer, dropping funnel and thermometer, add 500mL polyethylene glycol dropwise through the dropping funnel, start the stirrer at 400r / min After stirring for 30 minutes at a rotating speed, move it into an ultrasonic disperser, ultrasonically disperse with a power of 300W for 2 hours, and then concentrate it to 2 / 3 of ...
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