Polarizing plate with pressure-sensitive adhesive layer
A pressure-sensitive adhesive layer and pressure-sensitive adhesive technology, applied in the field of polarizers, can solve the problems of poor followability of polarizer height differences, difficulty in pasting polarizers, poor appearance, etc., to prevent abnormal appearance and prevent peeling. Effect
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Examples
Embodiment 1
[0142] Polarizing plate production
[0143] (Preparation of pressure sensitive adhesive)
[0144] The solution containing the (meth)acrylic polymer (B-1) obtained in Production Example 6 and 0.1 parts by weight of trimethylolpropane xylylene diisocyanate relative to 100 parts by weight of the solid content of the solution (Manufactured by Mitsui, Inc., trade name: "TAKENATED110N"), and 0.3 parts by weight of dibenzoyl peroxide as a crosslinking agent and 0.1 parts by weight of γ-glycidoxypropyl as a silane coupling agent Methoxysilane (manufactured by Shin-Etsu Chemical Co., Ltd., trade name: "KBM-403") is compounded. Thus, a pressure-sensitive adhesive solution was obtained.
[0145] (Production of polarizing plate with pressure-sensitive adhesive layer)
[0146] Using a fountain coater, uniformly apply the resulting pressure-sensitive adhesive solution to the surface of a polyethylene terephthalate film (substrate) treated with a silicone-based release agent , And dry for 2 min...
Embodiment 2 to 8
[0148] Polarizing plate production
[0149] Except that: those shown in Table 1 were used as a laminate including a polarizing film and a protective film, a (meth)acrylic polymer, and a crosslinking agent; and the thickness of the pressure-sensitive adhesive layer was set as shown in Table 1. Except for the thickness shown, a polarizing plate having a pressure-sensitive adhesive layer was each obtained in the same method as in Example 1. It should be noted that in Example 8, when the pressure-sensitive adhesive solution was produced, lithium trifluoromethanesulfonylimide (manufactured by Morita Chemical Industries Co., Ltd.) was compounded as an antistatic agent.
[0150]
reference example 1
[0165] Except that: Laminate A-4 was used instead of Laminate A-1; and the pressure-sensitive adhesive layer was transferred to the protective film, a polarizing plate (protective film (40 μm) was obtained in the same manner as in Example 1 / Polarizing film (20 μm) / Protective film (40 μm) / Pressure sensitive adhesive layer (20 μm)).
[0166]
[0167] The following evaluations were performed on the optical laminates or the polarizing plates having a pressure-sensitive adhesive layer obtained in Examples, Comparative Examples, and Reference Examples. The results are shown in Table 2.
[0168] (The amount of creep of the pressure-sensitive adhesive layer)
[0169] The end of a polarizing plate with a pressure-sensitive adhesive layer cut into a size of 10mm wide by 50mm long (with a size of 10mm wide by 10mm long) was pasted to the stainless steel plate via the pressure-sensitive adhesive layer and kept at 50°C The resultant was treated in an autoclave at 5 atmospheres for 15 minu...
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Abstract
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