Method for preparing electrode from natural graphite
A natural graphite, electrode preparation technology, applied in battery electrodes, circuits, electrical components, etc., can solve the problems of small specific surface area, complex electrode production process, etc., to increase specific surface area, improve electrode stability and activity, and easily conduct network. The effect of the passage
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Embodiment 1
[0030] The first step: preparation of high-grade graphite products
[0031] Liaoning graphite mine, raw ore grade is 8.69%, other element analysis is as follows:
[0032]
[0033] 1. Take 400g of graphite raw ore, grind the ore for 4 minutes under the condition of grinding concentration of 65%, put the ground ore in a 1.5L flotation tank for 5 minutes of flotation; and regrind the roughed ore concentrate three times The re-election process, the grinding time is 6min, 8min, 10min respectively, and the flotation time is: 7min, 4min, 4min; the obtained concentrate grade is 90.88%.
[0034] 2. Take 20g of flotation concentrate, add NaOH solution with a concentration of 15% according to the liquid-solid ratio of 3:1, react in an autoclave at 180°C for 4 hours, and filter to obtain the filter residue.
[0035] 3. Get 10g of the ore (filter residue obtained in step 2) after high-pressure alkali leaching, add a concentration of 60% NaOH solution according to the alkali-mine ratio ...
Embodiment 2
[0047] The first step: preparation of high-grade graphite products
[0048] Amu Beach Graphite Mine, raw ore grade is 10.42%, other element analysis is as follows:
[0049]
[0050] 1. Take 400g of graphite raw ore, grind the ore for 4 minutes under the condition of grinding concentration of 65%, put the ground ore in a 1.5L flotation tank for 5 minutes of flotation; and regrind the roughed ore concentrate three times The re-election process, the grinding time is 6min, 8min, 10min respectively, and the flotation time is: 7min, 4min, 4min; the obtained concentrate grade is 91.95%.
[0051] 2. Take 20g of flotation concentrate, add NaOH solution with a concentration of 15% according to the liquid-solid ratio of 3:1, react in an autoclave at 180°C for 4 hours, and filter to obtain the filter residue.
[0052]3. Get 10g of the ore (filter residue obtained in step 2) after high-pressure alkali leaching, add a concentration of 60% NaOH solution according to the alkali-mine ratio...
Embodiment 3
[0064] The first step: preparation of high-grade graphite products
[0065] Liaoning graphite mine, raw ore grade is 8.69%, other element analysis is as follows:
[0066]
[0067]
[0068] 1. Take 400g of graphite raw ore, grind the ore for 5 minutes under the condition of grinding concentration of 55%, put the ground ore into a 1.5L flotation tank for flotation for 5 minutes; and regrind the roughed ore concentrate three times The re-election process, the grinding time is 6min, 8min, 10min respectively, and the flotation time is: 7min, 4min, 4min; the grade of the obtained concentrate is 90.74%.
[0069] 2. Take 20g of flotation concentrate, add 10% ammonia water at a liquid-solid ratio of 5:1, react in an autoclave at 200°C for 1 hour, and filter to obtain a filter residue.
[0070] 3. Take 10 g of the ore after high-pressure alkali leaching (the filter residue obtained in step 2), add ammonia water with a concentration of 50% according to the alkali-mineral ratio of ...
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