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A Heat-resistant Rare Earth Magnesium Alloy and Its Heat Treatment Process for Castings with Uneven Wall Thickness

A rare earth magnesium, uniform technology, applied in the field of heat treatment of magnesium alloy materials, can solve the problems of uneven heating, high temperature strength can not meet the requirements of use, different precipitation temperature and peak precipitation time, etc., to achieve the effect of simple and easy process

Active Publication Date: 2017-07-11
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, using the existing heat treatment system to heat treat large and complex Mg–Y–Nd series rare earth magnesium alloy castings for aviation and aerospace, due to the large difference in thickness at each position of the casting, the heating process is uneven at each position, and the alloy The type and structure of the precipitation strengthening phase are different, and the corresponding suitable precipitation temperature and peak precipitation time are also different, resulting in uneven size of the precipitated phase, and finally manifested as uneven mechanical properties of the thin-walled and thick-walled castings after heat treatment. Even the high temperature strength cannot meet the requirements of use, and the disadvantages of low plasticity

Method used

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  • A Heat-resistant Rare Earth Magnesium Alloy and Its Heat Treatment Process for Castings with Uneven Wall Thickness
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  • A Heat-resistant Rare Earth Magnesium Alloy and Its Heat Treatment Process for Castings with Uneven Wall Thickness

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Experimental program
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Embodiment 1

[0041] In this embodiment, the composition (wt.%) is: Y 3.4-3.8; Nd 2.6-3.0; Ag 0.5-0.6; Zr 0.4-0.5; 10-60mm, outer diameter of upper bottom surface 290-300mm, outer diameter of lower bottom surface 750-850mm, height 400-450mm, and Mg-Y-Nd-Ag series rare earth magnesium alloy castings with complex oil and gas pipelines as raw materials. First, the surface of the magnesium alloy casting is mechanically polished to remove the sand and oxide layer on the surface, and then cleaned with chromate; then, the obtained magnesium alloy casting is placed in a resistance furnace, and the temperature is raised to 530°C with the furnace, and the heating time is After 9 hours of heat preservation, the furnace is cooled by strong wind. The time for the casting to be transferred from the solid solution resistance furnace to the strong wind quenching equipment is controlled within 30s. The cooling rate of the casting is 100°C / min; In the furnace, the temperature was raised to 220°C with the fur...

Embodiment 2

[0043] In this embodiment, the composition (wt.%) is: Y 3.4-3.8; Nd 2.6-3.0; Ag 0.5-0.6; Zr 0.4-0.5; 10-60mm, outer diameter of upper bottom surface 290-300mm, outer diameter of lower bottom surface 750-850mm, height 400-450mm, and Mg-Y-Nd-Ag series rare earth magnesium alloy castings with complex oil and gas pipelines as raw materials. First, the surface of the magnesium alloy casting is mechanically polished to remove the sand and oxide layer on the surface, and then cleaned with chromate; then, the obtained magnesium alloy casting is placed in a resistance furnace, and the temperature is raised to 535°C with the furnace, and the heating time is 3h15min, after 8h of heat preservation, strong wind cooling out of the furnace, the time for the casting to be transferred from the solid solution resistance furnace to the strong wind quenching equipment is controlled within 30s, and the cooling rate of the casting is 120°C / min; then the cooled magnesium alloy casting is placed in th...

Embodiment 3

[0045] In this embodiment, the composition (wt.%) is: Y 3.4-3.8; Nd 2.6-3.0; Ag 0.5-0.6; Zr 0.4-0.5; 10-60mm, outer diameter of upper bottom surface 290-300mm, outer diameter of lower bottom surface 750-850mm, height 400-450mm, and Mg-Y-Nd-Ag series rare earth magnesium alloy castings with complex oil and gas pipelines as raw materials. First, the surface of the magnesium alloy casting is mechanically polished to remove the sand and oxide layer on the surface, and then cleaned with chromate; then, the obtained magnesium alloy casting is placed in a resistance furnace, and the temperature is raised to 540°C with the furnace, and the heating time is 3h30min, after 6h of heat preservation, strong wind cooling out of the furnace, the time for the casting to be transferred from the solid solution resistance furnace to the strong wind quenching equipment is controlled within 30s, and the cooling rate of the casting is 120°C / min; then the cooled magnesium alloy casting is placed in th...

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Abstract

The invention discloses heat-resisting rare earth magnesium alloy and a thermal treatment process for an uneven-wall-thickness casting of the heat-resisting rare earth magnesium alloy. The heat-resisting rare earth magnesium alloy is composed by Y, Nd, Ag, Zr, Gd, and the balance Mg and inevitable impurity elements. The thermal treatment process includes the steps that the uneven-wall-thickness heat-resisting rare earth magnesium alloy casting of a complex structure is heated to 530-540 DEG C, and after heat preservation and solid solution, the casting is cooled to the room temperature at the speed of 90 DEG C / min or more; and then the casting is heated to 220-230 DEG C, and after heat preservation and artificial aging, the casting is discharged out of a furnace and air-cooled. The heat-resisting rare earth magnesium alloy is reasonable in component ratio, the process is simple, and operation is convenient; during implementation, only conventional thermal treatment equipment is needed, the technological process is simple, practicable, safe and reliable, and the thermal treatment process is suitable for treating large-size rare earth magnesium alloy castings which are complex in shape and have differences in wall thickness; a feasible scheme is provided for improving the performance of the complex-structure rare earth magnesium alloy castings for aviation and spaceflight, the using requirements for parts of the field of aviation and spaceflight are met, and industrial production is facilitated.

Description

technical field [0001] The invention belongs to the technical field of heat treatment of magnesium alloy materials, and relates to a heat treatment process of a heat-resistant rare earth magnesium alloy and castings with uneven wall thickness thereof, in particular to the heat treatment of Mg-Y-Nd-Ag series rare earth magnesium alloy castings. Background technique [0002] Mg–Y–Nd alloys are one of the typical representatives of rare earth magnesium alloys. Due to the multiple effects of rare earth elements, Mg 24 Y 5 , Mg 2 Y, Mg 41 Nd 5 and Mg 14 Nd 2 Compounds such as Y have good heat resistance and high strength, and are widely used in the manufacture of structural devices that require high temperature service in the fields of aviation and aerospace. At present, the rare earth magnesium alloy structural parts used in aviation and aerospace are mostly formed by low-pressure casting for large size, complex shape, and different wall thickness. Segregation forms a lar...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C23/06C22F1/06
CPCC22C23/06C22F1/06
Inventor 李慧中姚三成梁霄鹏吕凤赵俊刚
Owner CENT SOUTH UNIV