Microwave vacuum freeze-drying method for Dendrobium officinale
A technology of Dendrobium candidum and drying method, which is applied in the direction of drying solid materials, types of dried products, and drying solid materials without heating, etc., can solve the effects of effective physiologically active active ingredients, uneven heating of Dendrobium candidum, deterioration of sensory indicators, etc. problems, achieve the effects of shortening the sublimation time, improving storage stability, and fast drying speed
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Embodiment 1
[0018] A method for microwave vacuum freeze-drying of dendrobium officinale comprises the following steps:
[0019] (1) Pretreatment: wash Dendrobium officinale and drain the surface moisture, then fumigate with steam for 5min and then cool to room temperature;
[0020] (2) Pre-freezing and freezing: putting the pretreated Dendrobium officinale into a freezer with a storage temperature of -36°C to quickly cool down the Dendrobium candidum to the storage temperature within 30 minutes, and then freeze at the constant temperature for 3 hours at the storage temperature;
[0021] (3) Sublimation: place the frozen Dendrobium candidum in a vacuum chamber with a temperature of -45°C and a vacuum of 30Pa, and turn on the microwave generator to sublimate for 1 hour at a modulation power of 250W / Kg;
[0022] (4) Desorption drying: dry for 3 hours at a temperature of 40°C and a vacuum of 0.3mPa;
[0023] (5) Post-processing: the dried Dendrobium candidum is graded, packaged and sealed. ...
Embodiment 2
[0025] A method for microwave vacuum freeze-drying of dendrobium officinale comprises the following steps:
[0026] (1) Pretreatment: wash Dendrobium officinale and drain the surface moisture, then fumigate with steam for 3 minutes and then cool to room temperature;
[0027] (2) Pre-freezing and freezing: putting the pretreated Dendrobium candidum into a freezer with a storage temperature of -32°C to quickly cool down the Dendrobium candidum to the storage temperature within 30 minutes, and then freeze at the constant temperature for 3 hours at the storage temperature;
[0028] (3) Sublimation: place frozen Dendrobium candidum in a vacuum chamber with a temperature of -40°C and a vacuum of 13Pa, and turn on the microwave generator to sublimate for 2 hours at a modulation power of 200W / Kg;
[0029] (4) Desorption drying: dry for 3 hours at a temperature of 30°C and a vacuum of 0.15mPa;
[0030] (5) Post-processing: the dried Dendrobium candidum is graded, packaged and sealed. ...
Embodiment 3
[0032] A method for microwave vacuum freeze-drying of dendrobium officinale comprises the following steps:
[0033] (1) Pretreatment: wash Dendrobium officinale and drain the surface moisture, then fumigate with steam for 4min and then cool to room temperature;
[0034] (2) Pre-freezing and freezing: putting the pretreated Dendrobium officinale into a freezer with a storage temperature of -35°C to quickly cool down the Dendrobium candidum to the storage temperature within 30 minutes, and then freeze at the constant temperature for 3 hours at the storage temperature;
[0035] (3) Sublimation: place the frozen Dendrobium officinale in a vacuum chamber with a temperature of -42°C and a vacuum of 25Pa, and turn on the microwave generator to sublimate for 1 to 2 hours at a modulation power of 220W / Kg;
[0036] (4) Desorption drying: dry for 2 hours at a temperature of 35°C and a vacuum of 0.2mPa;
[0037] (5) Post-processing: the dried Dendrobium candidum is graded, packaged and s...
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