Photosensitive resin composite and application thereof
A technology of photosensitive resin and composition, applied in optics, optomechanical equipment, instruments, etc., which can solve problems such as resolution and taper angle acceptance
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example 1
[0243]Production Example 1: Production method of diol compound (a-1-1) containing polymerizable unsaturated group
[0244] With 100 parts by weight of fluorene epoxy compound (model ESF-300, manufactured by Nippon Steel Chemical; epoxy equivalent 231), 30 parts by weight of acrylic acid, 0.3 parts by weight of benzyltriethylammonium chloride, 0.1 parts by weight of 2,6-di-tert-butyl-p-cresol and 130 parts by weight of propylene glycol monomethyl ether acetate are added to a 500-ml four-necked flask in a continuous addition mode; the feed rate is controlled at 25 parts by weight / minute, and the reaction The temperature of the process is maintained at 100°C to 110°C. After 15 hours of reaction, a light yellow transparent mixed liquid with a solid content concentration of 50% by weight can be obtained; then, the above light yellow transparent mixed liquid is extracted, filtered, heated and dried step, the polymerizable unsaturated group-containing diol compound (a-1-1) of Prepara...
preparation example 2
[0245] Production Example 2: Production method of diol compound (a-1-2) containing polymerizable unsaturated group
[0246] 100 parts by weight of fluorene epoxy compound (model PG-100, manufactured by Osaka Gas; epoxy equivalent 259), 35 parts by weight of methacrylic acid, 0.3 parts by weight of benzyltriethylammonium chloride, 0.1 parts by weight of 2,6-di-tert-butyl-p-cresol and 135 parts by weight of propylene glycol monomethyl ether acetate are added to a 500-ml four-necked flask in a continuous addition mode; the feed rate is controlled at 25 parts by weight / minute, and the reaction process The temperature is maintained at 100°C to 110°C, and after 15 hours of reaction, a light yellow transparent mixed liquid with a solid content of 50% by weight can be obtained; the above light yellow transparent mixed liquid is subjected to the steps of extraction, filtration and heating and drying , the polymerizable unsaturated group-containing diol compound (a-1-2) of Preparation E...
preparation example 3
[0247] Production Example 3: Production method of diol compound (a-1-3) containing polymerizable unsaturated group
[0248] With 100 parts by weight of fluorene epoxy compound (model ESF-300, manufactured by Nippon Steel Chemical; epoxy equivalent 231), 100 parts by weight of 2-methacryloylethoxysuccinate, 0.3 parts by weight of chlorine Benzyltriethylammonium, 0.1 parts by weight of 2,6-di-tert-butyl-p-cresol and propylene glycol monomethyl ether acetate of 200 parts by weight are added to a 500-milliliter four-necked flask in a continuous addition mode; The speed is controlled at 25 parts by weight / minute, and the temperature of the reaction process is maintained at 100°C to 110°C. After 15 hours of reaction, a light yellow transparent mixed solution with a solid content of 50% by weight can be obtained; the above light yellow is transparent The mixed solution was subjected to the steps of extraction, filtration, and heating and drying to obtain the diol compound (a-1-3) con...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More 