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Method for preparing thermochromic intelligent glass

A smart glass and thermochromic technology, applied in the field of thermochromic smart glass preparation, can solve the problems of high energy consumption, difficult to guarantee the quality and performance of thermochromic coatings, and high equipment investment

Active Publication Date: 2016-07-27
GUANGZHOU INST OF ENERGY CONVERSION - CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The purpose of the present invention is to provide a method for preparing thermochromic smart glass, which solves or improves the poor safety performance of glass substrates, difficulty in guaranteeing the quality and performance of thermochromic coatings, and problems in existing thermochromic smart glass preparation methods. For the problems of high equipment investment and high energy consumption, aiming at the annealing process in the preparation of thermochromic smart glass, the characteristics of high radiation heating efficiency of the lamp tube are maximized to provide a suitable heating method for the glass substrate during annealing treatment, thereby shortening the annealing process. The heating time of the treatment can realize the crystallization modification of the thermochromatic coating

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  • Method for preparing thermochromic intelligent glass
  • Method for preparing thermochromic intelligent glass
  • Method for preparing thermochromic intelligent glass

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Experimental program
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Embodiment 1

[0054] The preparation method of the thermochromic smart glass provided in this embodiment 1 is based on figure 1 implemented by the heat treatment device. In this embodiment 1, the power density of the heat radiation lamp tube in the preheating section and the annealing section is 120kw / m 2 , the substrate used is 4mm toughened glass ordinary transparent float glass.

[0055] Such as figure 1 The shown heat treatment device includes a working platform, along the flow direction of the substrate heat treatment process, the working platform includes a preheating section 1 , an annealing section 2 and a cooling air grid section 3 in sequence. The working platform is provided with a transmission mechanism that runs through the entire working platform. In the present embodiment 1, the transmission mechanism is composed of several transmission roller tables 4 . Each of the preheating section 1, the annealing section 2 and the cooling grid section 3 is provided with one or more d...

Embodiment 2

[0087] The difference between the present embodiment 2 and the comparative example 6 in the embodiment 1 is that, as Figure 4 As shown, the length of the radiation lamp tube area 6 in the preheating section is greater than the length of the radiation lamp tube area 7 in the annealing section.

[0088] In this embodiment 2, use Figure 4 The arrangement of the shown annealing device for the preparation of thermochromic smart glass is as follows:

[0089] A) After the glass is cleaned, put it into the vacuum coating work area;

[0090] B) In the vacuum coating working area, the sputtering preparation process is adopted. First, the SiAl target is used to coat the SiNx film on the glass substrate, and the metal V target is used to coat the Ar and O 2 After the vanadium dioxide amorphous film was deposited on the SiNx film in the atmosphere, the NiCr film was deposited on the vanadium dioxide amorphous film in the Ar atmosphere by using a metal NiCr target, and then SiAl was use...

Embodiment 3

[0098] The difference between this embodiment 3 and embodiment 2 is that in this embodiment 3, the annealing treatment of the glass substrate is completed in a vacuum environment, and the glass substrate after the annealing treatment is cooled by a liquid non-contact method. Cooling is completed in the cooling chamber. Such as Figure 5 As shown, the cooling cavity includes an inner cavity 19 and an outer wall 20 , a cooling interlayer 21 for flowing coolant is provided between the inner cavity 19 and the outer wall 20 , and a heat-absorbing coating 22 is also coated on the inner surface of the inner cavity.

[0099] After heating, the surface temperature of the glass substrate reaches about 500°C, and it radiates infrared rays by itself. The radiated infrared rays are absorbed by the inner cavity, and the absorbed infrared rays (that is, the corresponding heat generated) are carried by the coolant in the cooling interlayer 21 through the cavity wall. At the same time, the gl...

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Abstract

The invention discloses a method for preparing thermochromic intelligent glass. The method is mainly characterized in that during annealing treatment, substrate glass sequentially passes through a preheating section and an annealing section, and heat radiation lamp tubes in the preheating section and the annealing section control own make and break according to the position state of the substrate glass so as to achieve alternate heating. Through producing the thermochromic intelligent glass by using the method disclosed by the invention, the energy consumption of a production process is lower; and by the method, a thermochromic coating of the glass can achieve the aim of crystallizing modification for a thermochromic functional layer, obvious oxidation metamorphism is avoided, and meanwhile, properties such as overall safety of the glass are satisfactory.

Description

technical field [0001] The invention relates to a method for preparing glass, in particular to a method for preparing thermochromic smart glass. Background technique [0002] Thermochromic smart glass is a kind of energy-saving coated glass that can automatically adjust the amount of light through the ambient temperature and light intensity, and intelligently control the indoor temperature. It is suitable for doors and windows of buildings and vehicles to reduce the power consumption of air conditioning and lighting. This kind of coated glass has multiple functions, including high thermal insulation properties, anti-static, UV absorption and photocatalyst etc. [0003] For the mass production of thermochromic smart glass, there are two traditional preparation process routes, namely chemical spraying thermal decomposition and sputtering coating. The thermal decomposition of chemical spraying has certain limitations due to the control of glass appearance color, film thickness...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C17/23
Inventor 徐刚詹勇军史继富肖秀娣
Owner GUANGZHOU INST OF ENERGY CONVERSION - CHINESE ACAD OF SCI