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Enzymatic secondary cycle injection liquefaction process and liquefaction system

A technology of jet liquefaction and secondary circulation, used in biochemical instruments, biochemical cleaning devices, enzyme production/bioreactors, etc., can solve the problems of short shelf life, waste of steam energy, unqualified liquefaction liquid, etc., to improve liquefaction efficiency , The effect of saving production costs and reducing equipment investment

Active Publication Date: 2021-08-03
广西金冠食品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Because the feed liquid recovered by the first spray flash evaporation is basically pasty, although adding enzyme preparation in the feed liquid recovery tank can reduce the viscosity of the paste after stirring, but still entraining a large amount of Unliquefied starch granules and agglomerated granules lead to low heat preservation and liquefaction efficiency in subsequent laminar flow tanks, which increases the difficulty of decomposing insoluble particles in the terminal secondary spraying
In order to improve the efficiency of the secondary injection, the temperature of the secondary injection must be increased to 145°C. This will not only cause waste of steam energy, but also cause unqualified liquefied liquid due to improper operation. The blue color of iodine reaction indicates that there is unhydrolyzed liquefied liquid in the liquefied liquid. The presence of starch causes difficulties in the post-saccharification section and increases the difficulty of filtration. The final product produced is easy to be turbid and has a short shelf life.

Method used

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  • Enzymatic secondary cycle injection liquefaction process and liquefaction system
  • Enzymatic secondary cycle injection liquefaction process and liquefaction system

Examples

Experimental program
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Effect test

Embodiment 1

[0019] A kind of enzymatic secondary cycle injection liquefaction process, it comprises the following steps:

[0020] 1) Mixing: adding high temperature resistant α-amylase to starch emulsion to form starch slurry;

[0021] 2) Primary spray liquefaction: send the starch slurry into the first liquefaction injector for 5 minutes of primary spray liquefaction, and the temperature of the primary spray liquefaction is 105°C;

[0022] 3) One-time flash evaporation: The feed liquid after the first spray liquefaction is flashed in the flash tank, and the flash evaporated feed liquid is sent to the feed liquid recovery tank for the second enzyme addition and stirring operation;

[0023] 4) Secondary cycle injection liquefaction: When the material liquid in the material liquid recovery tank reaches the middle section of the material liquid recovery tank, the material liquid in the material liquid recovery tank is continuously pumped into the second liquefaction injector for secondary in...

Embodiment 2-5

[0026] Using the same preparation method as in Example 1, the difference is that the reaction temperature and time listed in Table 1 are used to replace the corresponding values ​​used in Example 1 for the steps of primary spray liquefaction, secondary cycle spray liquefaction and heat preservation discharge.

[0027] Table 1:

[0028]

[0029] The liquid part of the liquefied liquid obtained by the process of the present invention is clear and transparent, and the protein is separated and coagulated intact and floats on the surface of the liquefied liquid. The iodine reaction test of the liquefied liquid discharged from the laminar flow tank does not show blue, and the pass rate is 100%. Its DE value is 15-20, and the degree of liquefaction is high.

[0030] In the present invention, the feed liquid is pumped into the second liquefaction injector when the liquid in the feed liquid recovery tank rises to the middle section of the tank body. At this time, the viscosity of th...

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Abstract

The invention discloses an enzymatic secondary cycle injection liquefaction process and a liquefaction system, which changes the installation position of the second liquefaction injector in the traditional liquefaction system, and after the first injection liquefaction, the second injection liquefaction device directly extracts the material The feed liquid in the liquid recovery tank is sprayed and liquefied in the second cycle, and the feed liquid sprayed by the second liquefaction injector and the feed liquid sprayed by the first liquefaction injector are sent into the flash tank at the same time for flash mixing and dethickening, and then Send it into the feed liquid recovery tank for secondary enzyme mixing operation, until the liquid level in the feed liquid recovery tank reaches the set value, then pump the feed liquid in the feed liquid recovery tank into the laminar flow tank for heat preservation, at this time the feed liquid The liquid part of the feed liquid in the recovery tank is clear and transparent, while the protein is separated and condensed intact and floats on the surface of the liquefied liquid, which greatly improves the liquefaction efficiency of starch.

Description

technical field [0001] The invention relates to the technical field of starch sugar production, in particular to an enzymatic secondary cycle injection liquefaction process and a liquefaction system. Background technique [0002] Glucose production by enzymatic hydrolysis can be divided into two steps: the first step is to use liquefying enzymes to hydrolyze gelatinized starch into dextrin and oligosaccharides, etc., to reduce viscosity and increase fluidity, so it is called liquefaction in industry; the second step is to use Glucoamylase further hydrolyzes dextrin or oligosaccharides into glucose, which is called saccharification in production. [0003] The common liquefaction process is the secondary injection liquefaction method. The process is to adjust the pH value after mixing the starch milk, add enzyme preparations and stir evenly, then send it to the first liquefaction injector for one injection, and the injected material liquid enters the A flash evaporation is ca...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C12P19/14C12M1/40C12M1/02
CPCC12M21/18C12M23/58C12M27/02C12M29/06C12P19/14
Inventor 高锦荣
Owner 广西金冠食品有限公司