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Wide temperature range bio-lubricating oil for vehicles and preparation method thereof

A wide temperature range, lubricating oil technology, applied in the field of lubricating oil, can solve problems such as insufficient lubricating performance, achieve good lubricating effect, simple process, and reduce industrial production costs.

Active Publication Date: 2018-06-15
HEFEI UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The present invention aims at the current situation that the existing lubricating oil has insufficient lubricating performance in extreme high and low temperature environments, and the purpose is to provide a wide temperature range biological lubricating oil for vehicles and its preparation method, so as to improve the lubrication state of vehicles in extreme climates

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] (1) Add 0.4 part of dispersant to 50 parts of polyalphaolefin and mix evenly, then add 0.6 part of lubricant and 0.01 part of diphenylamine in sequence, heat up to 120°C and stir and mix for 20 minutes to obtain oil A;

[0025] (2) Add 0.8 part of dispersant to 47.7 parts of refined bio-oil and mix well, then add 0.3 part of poly C14 alkyl methacrylate and 0.19 part of T613 ethylene-propylene copolymer in turn, raise the temperature to 65°C and stir to get oil B;

[0026] (3) Slowly add oil B dropwise to oil A at 80°C, keep stirring for 10 minutes, then lower the temperature of the system to -20°C, continue to keep stirring for 20 minutes, then warm up to room temperature, centrifuge at 2000rpm for 5 minutes, and take the upper layer The oil is a wide temperature range bio-lubricating oil for vehicles.

Embodiment 2

[0028] (1) Add 1.5 parts of dispersant to 58.7 parts of polyalphaolefin and mix well, then add 2 parts of lubricant and 0.1 part of 2,6-di-tert-butyl-4-methylphenol in sequence, heat up to 140°C and stir and mix 30min, get oil A;

[0029] (2) Add 1 part of dispersant to 34 parts of refined bio-oil and mix well, then add 0.5 parts of polymethacrylate C15 alkyl ester and 2.2 parts of T613 ethylene-propylene copolymer in turn, heat up to 70 ° C and stir to obtain oil B;

[0030] (3) Slowly add oil B dropwise to oil A at 80°C, keep stirring for 15 minutes, then lower the temperature of the system to -20°C, continue to keep stirring for 20 minutes, then warm up to room temperature, centrifuge at 2000rpm for 5 minutes, and take the upper layer The oil is a wide temperature range bio-lubricating oil for vehicles.

Embodiment 3

[0032] (1) Add 0.8 parts of dispersant to 55 parts of polyalphaolefin and mix evenly, then add 1 part of lubricant and 0.2 parts of p-phenylenediamine in sequence, heat up to 130°C and stir and mix for 25 minutes to obtain oil A;

[0033] (2) Add 0.4 parts of dispersant to 40 parts of refined bio-oil and mix well, then add 0.5 parts of poly C16 alkyl methacrylate and 2.1 parts of T613 ethylene-propylene copolymer in turn, heat up to 70°C and stir to get oil B;

[0034] (3) Slowly add oil B dropwise to oil A at 85°C, keep stirring for 20 minutes, then lower the temperature of the system to -20°C, continue to keep stirring for 20 minutes, then warm up to room temperature, centrifuge at 2000rpm for 5 minutes, and take the upper layer The oil is a wide temperature range bio-lubricating oil for vehicles.

[0035] The wide-temperature-range bio-lubricating oil obtained in the above-mentioned examples was used in the automobile engine bench test, and the results showed that compared...

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Abstract

The invention discloses a wide-temperature-range biolubricant for a vehicle and a preparation method of the wide-temperature-range biolubricant. The biolubricant comprises components in parts by mass as follows: 92-99 parts of base oil, 0.5-3 parts of a lubricating agent, 0.01-0.2 parts of an antioxidant, 0.3-2 parts of a pour point depressant, 0.1-5 parts of a viscosity index improver and 0.08-3 parts of a dispersing agent, wherein the base oil is an oil mixture of poly-alpha-olefin and refined bio-oil. The preparation method of the biolubricant comprises following steps: part of the dispersing agent, the lubricating agent and the antioxidant are sequentially added to poly-alpha-olefin and subjected to heating, stirring and uniform mixing, and oil A is obtained; besides, the remaining dispersing agent, the pour point depressant and the viscosity index improver are sequentially added to the refined bio-oil and subjected to heating, stirring and uniform mixing, and oil B is obtained; finally, the oil B is slowly dropwise added to the oil A, an oil mixture is subjected to heating stirring, low-temperature stirring and normal-temperature centrifugal separation, and the biolubricant is obtained. The biolubricant is good in viscosity-temperature performance, environment-friendly and biodegradable, has good low-temperature starting performance for a vehicle engine, and can have a good lubricating effect in a wider temperature range.

Description

technical field [0001] The invention relates to the field of lubricating oil, in particular to a wide temperature range biological lubricating oil for vehicles and a preparation method thereof. Background technique [0002] With the popularization of domestic cars in our country, the lubrication problems related to cars have become increasingly prominent. Under normal circumstances, vehicles have a lubricating oil change cycle specified by the manufacturer. However, due to the impact of extreme weather in recent years, even if the vehicle is changed according to the requirements specified by the manufacturer, failures due to poor lubrication still emerge in endlessly, and sometimes even affect the vehicle. and personnel safety. Although there are some multi-grade lubricating oil products on the market at present, they are mainly equipped for conventional winter and summer temperatures. They are obviously insufficient for vehicle lubrication in extreme climates. , The fluid...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10M169/04C10N40/25C10N30/06C10N30/08
CPCC10M169/044C10M2201/041C10M2201/05C10M2203/003C10M2205/0206C10M2205/022C10M2205/024C10M2207/026C10M2207/126C10M2207/281C10M2209/084C10M2215/064C10M2215/066C10N2030/06C10N2030/08C10N2030/64C10N2040/25
Inventor 徐玉福彭玉斌郑晓静胡献国
Owner HEFEI UNIV OF TECH
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