A photosensitive composition, a cured membrane, a color filter, a display element, a solid shooting element, a touch screen and an LED illuminant body
A technology of photosensitive composition and hardened film, which is applied in the direction of optical filters, optical elements, and photosensitive materials used in optomechanical equipment, etc., and can solve the problems such as the inability to form fine patterns
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[0146] Next, the present invention will be specifically described by way of synthesis examples, examples, and comparative examples, but the present invention is not limited by these examples.
Synthetic example 1
[0147] [Synthesis Example 1] Synthesis of Alkali-Soluble Polymer Solution (A-1)
[0148] Into a four-necked flask equipped with a stirrer, diethylene glycol methyl ethyl ether (hereinafter abbreviated as "EDM"), methacrylic acid as the component (a1), and methacrylic acid as the component (a2) were charged with the following composition. Dicyclopentyl acrylate, N-cyclohexylmaleimide, and 2,2'-azobis(isobutyrate)dimethyl (hereinafter abbreviated as "V-601") as a polymerization initiator. V-601 is a trade name; Wako Pure Chemical Industries, Ltd.), and heating was performed at 115° C. for 3 hours.
[0149]
[0150] The solution after completion of the reaction was cooled to room temperature to obtain a 33.3% by weight solution of the alkali-soluble polymer (A-1). The weight average molecular weight determined by GPC analysis was 3,100.
[0151] Furthermore, the term "33.3% by weight solution of the alkali-soluble polymer (A-1)" here means the weight of the solid matter and ...
Synthetic example 2
[0152] [Synthesis Example 2] Synthesis of Alkali-Soluble Polymer Solution (A-2)
[0153] In a four-neck flask equipped with a stirrer, EDM, methacrylic acid as component (a1), dicyclopentyl methacrylate as component (a2), and methoxypolyethylene glycol were charged with the following composition. 400 methacrylate, N-cyclohexylmaleimide, and V-601 as a polymerization initiator were heated at 115° C. for 3 hours.
[0154]
[0155]
[0156] The solution after completion of the reaction was cooled to room temperature to obtain a 33.3% by weight solution of the alkali-soluble polymer (A-2). The weight average molecular weight determined by GPC analysis was 3,300.
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