Compound, and material and organic light-emitting device including same

A compound and aromatic compound technology, applied in the field of compounds, can solve the problems of power consumption, narrow viewing angle, slow display screen response rate, etc., and achieve the effects of good color coordinates, low driving voltage and high efficiency

Inactive Publication Date: 2016-10-05
EVERDISPLAY OPTRONICS (SHANGHAI) CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, its disadvantages such as slow response rate of the display screen, power consumption, and narrow viewing angle are not enough to become a perfect display screen.

Method used

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  • Compound, and material and organic light-emitting device including same
  • Compound, and material and organic light-emitting device including same
  • Compound, and material and organic light-emitting device including same

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038]

[0039] Add 0.1 mol of reactant A, 0.1 mol of reactant B, and 1000 mL of solvent toluene into the reaction flask, heated to reflux for 24 hours under nitrogen protection, cooled, removed toluene, added with dichloromethane, washed with water, dried, the crude product was passed through the column, and then used Dichloromethane and ethanol were recrystallized and purified to obtain the product compound 1. The MS and H-NMR characterization data are as follows.

[0040] MS: m / e=701.24 (M+H + ).

[0041] H-NMR (400M, CDCl 3 ): 7.53(2H d), 7.62(4H t), 7.71(4H t), 8.58(1H s), 7.67(1H s), 7.76(1H s), 7.34(2H d), 8.32(2H d), 7.34 (4Ht), 7.29 (2Hs), 1.61 (12Ht).

Embodiment 2

[0043]

[0044] Add 0.1 mol of reactant C, 0.3 mol of reactant B, and 1000 mL of solvent toluene into the reaction flask, heated to reflux for 24 hours under nitrogen protection, cooled, removed toluene, added with dichloromethane, washed with water, dried, the crude product was passed through the column, and then used Dichloromethane and ethanol were recrystallized and purified to obtain the product compound 6. The MS and H-NMR characterization data are as follows.

[0045] MS: m / e=804.28 (M+H + ).

[0046] H-NMR (400M, CDCl 3 ): 7.53(4Ht), 7.62(8Ht), 7.71(8Ht), 8.34(2Hd), 7.61(2Hd), 7.64(4Ht), 1.61(12Ht).

Embodiment 3

[0048]

[0049] Add 0.1 mol of reactant D, 0.1 mol of reactant E, and 1000 mL of solvent toluene into the reaction flask, heated to reflux for 24 hours under nitrogen protection, cooled, removed toluene, added with dichloromethane, washed with water, dried, the crude product was passed through the column, and then Recrystallization and purification with dichloromethane and ethanol gave the product compound 5, and its MS and H-NMR characterization data are as follows.

[0050] MS: m / e=765.27 (M+H + ).

[0051] H-NMR (400M, CDCl 3 ): 7.53(2H d), 7.62(4H t), 7.71(4H t), 7.58(2H d), 7.77(2H d), 7.79(2H d), 7.54(2H d), 7.64(1H s), 8.32(2Hd), 8.34(2Hd), 8.61(2Hd), 8.64(2Hd).

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Abstract

The invention provides a compound having the structure as follows, wherein the substituent groups R1 and R2 are both electron withdrawing groups. The invention also provides a material and an organic light-emitting device which include the compound. The organic light-emitting device has low driving voltage, high efficiency and good color coordinates and is more high-effective and energy-saving.

Description

technical field [0001] The present invention relates to a compound, in particular a compound that can be used for preparing organic electroluminescent devices. Background technique [0002] At present, the display is mainly based on TFT-LCD (thin film transistor type liquid crystal display), because the display is a non-self-luminous display, it must project light through the backlight, and sequentially penetrate the polarizer and glass in the TFT-LCD panel. Substrates, liquid crystal layers, color filters, glass substrates, polarizers and other related components, and finally enter the human eye for imaging to achieve the function of display. However, its display screen has shortcomings such as slow response rate, power consumption, and narrow viewing angle, which are insufficient to become a perfect display screen. [0003] With the development of the information age, organic electroluminescent devices (OLEDs) with high efficiency, energy saving and light weight have attr...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07F7/08C07F7/10H01L51/54
Inventor 杨红领
Owner EVERDISPLAY OPTRONICS (SHANGHAI) CO LTD
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