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Washing device of COD reflux condensing tube and washing method thereof

A technology for refluxing condenser tubes and cleaning devices, which is used in cleaning methods and utensils, chemical instruments and methods, and cleaning hollow objects, etc., can solve the problems of occupying the space of condenser tubes, affecting the condensation effect, and affecting the appearance, and saving the laboratory. cost, improve condensation effect, save cleaning cost

Inactive Publication Date: 2017-01-25
NANJING BAIYUN CHEM ENVIRONMENTAL MONITORING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] As a common environmental monitoring factor, COD is generally used for titration measurement by the potassium dichromate method during laboratory batch testing. The wall is easy to accumulate yellow-brown scale and microorganisms, especially in summer, when microorganisms grow rapidly and produce a large amount of moss, which not only affects the overall appearance, but also occupies the space of the condenser pipe, reduces the water flow in the pipe, and seriously affects the condensation effect , leading to high COD results; second, titration produces a large amount of waste acid;
[0003] In actual work, the number of samples is large, and it is necessary to ensure the cleaning of the condensing device, improve the condensation effect of condensed water, and improve the accuracy of COD measurement. However, there has been no cleaning method with low cost, simple operation and good effect. relevant reports

Method used

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  • Washing device of COD reflux condensing tube and washing method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] see figure 1 , a COD reflux condensation tube cleaning device, including an iron frame 2 placed on the test bench 1, six condensation tubes 5 fixed on the iron frame at intervals side by side, starting from the outermost condensation tube on one side, the connection of the upper end of the outer tube The port is connected to the connection port at the lower end of the outer tube of the next adjacent condenser tube through the first silicone tube 6, and connected in this way until the connection port at the upper end of the penultimate condenser tube is connected to the outermost condensation tube on the other side through the fifth silicone tube. The connection port at the lower end of the outer tube is connected, and the connection port at the lower end of the outermost condenser tube that is not connected with the silicone tube is connected with a two-way pipe joint, and one of the two-way pipe joints passes through the connecting pipe and the waste liquid collector 8 ...

Embodiment 2

[0022] A method for cleaning the COD reflux condenser by utilizing the above-mentioned device, comprising the following steps:

[0023] 1) When the pipe clamp of the water inlet pipe 10 is clamped and the pipe clamp of the water outlet pipe 11 is opened at the same time, the waste acid solution (solution in the Erlenmeyer flask 4) that has been tested for COD is continuously poured into the waste water Liquid collector 8, using the principle of pressure difference and the continuity of water flow, injects the waste acid liquid into the condensation pipe 5, and after the waste acid liquid is filled to the outer pipes of all the condensation pipes 5, clamp the pipe clamp of the outlet pipe 11 Tight, utilize waste acid liquid to soak condenser pipe 5;

[0024] 2) After soaking, open the pipe clamp of the outlet pipe 11 to let the waste acid flow into the waste liquid pool, then open the pipe clamp of the water inlet pipe 10, turn on the faucet, and clean the condenser pipe 5 with...

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Abstract

The invention discloses a washing device of COD reflux condensing tube, comprising an iron support placed on the experiment table, an N condensing tube fixed on the iron support with abreast interval, wherein the N is no less than 2, connector at the bottom of outermost condensing outer tube not connecting with silicone tube is under connection with a bipass joint, and one path of the bipass joint is connected with liquid waste collector via connecting pipe, and the liquid waste collector height is 30-50cm higher than the top condensing tube, the other path in the bipass joint is connected with faucet via water inlet, connector at the upper end of outermost condensing outer tube not connecting with silicone tube is under connection with liquid waste tank via discharging tube, water inlet and discharging tube are respectively arranged with pipe clamp. The invention further discloses a method of using the above devices to wash COD reflux condensing tube; the method recycles the detected COD acid pickle to clean condensing tube, which improves condensation effect of reflux condensed water, thus improving accuracy of COD determination.

Description

technical field [0001] The invention relates to a COD reflux condensation pipe cleaning device and a cleaning method. Background technique [0002] As a common environmental monitoring factor, COD is generally used for titration measurement by the potassium dichromate method during laboratory batch testing. The wall is easy to accumulate yellow-brown scale and microorganisms, especially in summer, when microorganisms grow rapidly and produce a large amount of moss, which not only affects the overall appearance, but also occupies the space of the condenser pipe, reduces the water flow in the pipe, and seriously affects the condensation effect , leading to high COD results; second, titration produces a large amount of waste acid; [0003] In actual work, the number of samples is large, and it is necessary to ensure the cleaning of the condensing device, improve the condensation effect of condensed water, and improve the accuracy of COD measurement. However, there has been no ...

Claims

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Application Information

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IPC IPC(8): B08B9/027
CPCB08B9/027
Inventor 胡家富王秋艳俞新培王慧潘薇王璇
Owner NANJING BAIYUN CHEM ENVIRONMENTAL MONITORING
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