Laser continuous preparation method for nano graphite particles under effect of limiting layer

A technology of nano-graphite and graphite particles, applied in nanotechnology, chemical instruments and methods, inorganic chemistry, etc., can solve the problem of high cost and achieve the effect of low cost, low density and significant economic value

Active Publication Date: 2017-02-22
GUANGDONG UNIV OF TECH
View PDF5 Cites 4 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, for the direct use of pulsed laser ablation, there are certain requirements for the laser equipment used. Generally, ultrashort pulse lasers or high-power nanosecond lasers are required, so the cost of equipment is relatively high.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Laser continuous preparation method for nano graphite particles under effect of limiting layer
  • Laser continuous preparation method for nano graphite particles under effect of limiting layer
  • Laser continuous preparation method for nano graphite particles under effect of limiting layer

Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0033] The schematic diagram of the experimental device of the present invention is as figure 1 As shown, a laser continuous preparation method of nano-graphite particles under the action of a confinement layer, specifically comprises the following steps:

[0034] (1) First place the graphite sheet target 2 on the top of the workbench 1;

[0035] (2) Then change the glass confinement layer 3 above the graphite sheet target material 2, and ensure that the two are closely bonded together;

[0036] (3) Set the 4 parameters of the pulsed laser, among which, the power is 18W, the repetition frequency is 25kHz, the pulse width is 100ns, the number of scans is 2000 times, and the scanning method is galvanometer filling scanning. Focusing the pulse laser 4 through the lens 5 on the interface between the graphite sheet target 2 and the glass confinement layer 3, scanning, filling and ablation the graphite sheet target 2, so that the surface material of the graphite sheet target 2 is h...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
particle diameteraaaaaaaaaa
Login to view more

Abstract

The present invention provides a laser continuous preparation method for nano graphite particles under the effect of a limiting layer. The method comprises the steps of 1) placing the target material of a graphite sheet on a working table; 2) attaching a limiting layer to be above the graphite sheet; 3) focusing the pulse laser at the interface of the target material of the graphite sheet and the limiting layer and subjecting the target material of the graphite sheet to scanning, filling and ablation; 4) under the effect of the limiting layer, pushing obtained graphite particles into a liquid flow transport corridor through the impact action of laser-induced plasmas, wherein the particles are conveyed into a container by the liquid flow; 5) drying the solution in the container to obtain nano-sized graphite particles. According to the invention, no expensive equipment is adopted. Nano graphite particles, resistant to high temperature, good in electrical conductivity and thermal conductivity, excellent in lubricating property and good in chemical stability, can be obtained through the simply operated laser ablation process of inexpensive carbon raw materials under the effect of the limiting layer. Therefore, the method has a wide application prospect in related fields.

Description

technical field [0001] The invention belongs to the technical field of carbon nanomaterial preparation, and in particular relates to a laser continuous preparation method of nano-graphite particles under the action of a confining layer. Background technique [0002] In recent years, nano-carbon materials have been one of the focus and hotspots of scientific research. At present, most of the major research focuses on carbon nanotubes, nano-carbon fibers and super activated carbon, while further research on nano-graphite particles remains to be done. Compared with ordinary substances, nanoparticles have many new characteristics due to their small size and large specific surface area. These new characteristics will bring great inspiration and revolutionary influence to future industrial applications and scientific research. [0003] The study found that for nano-graphite particles, it is a good solid lubricant. In addition, because nano-graphite is stable and has certain adsorp...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C01B32/205B82Y40/00
CPCC01P2002/72C01P2002/85C01P2004/03C01P2004/62C01P2004/64
Inventor 谢小柱江伟魏昕胡伟任庆磊
Owner GUANGDONG UNIV OF TECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products