Four-channel fluorogenic quantitative PCR detection method and kit for combined detection of avian influenza H7N9 and H9N2
A fluorescent quantitative and combined detection technology, applied in biochemical equipment and methods, DNA/RNA fragments, recombinant DNA technology, etc., can solve difficult problems, achieve high accuracy, avoid missed diagnosis and misdiagnosis, sensitivity and specificity enhanced effect
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Embodiment 1
[0050] 1. Design of specific primers and probes
[0051] According to the nucleic acid sequences of H1-H16 and N1-N9 of avian influenza virus (Avian influenza virus), primers and probes (synthesized at Life Technology Company) for detection of avian influenza virus H7N9 and H9N2 genes were designed. Its sequence is as follows:
[0052]
[0053] 2. Specimen collection and pretreatment
[0054] The applicable specimen types of the method and the kit include poultry tissue, serum, throat swab, excreta, etc. Tissue samples: Take about 100-200 mg of tissue under sterile conditions, put it into a 1.5ml clean EP tube, and store it for testing. Serum: Take 3-5ml of venous blood from the tested bird with a disposable sterile syringe, keep the serum, and save it for testing. Pharyngeal and cloacal swabs: Use a cotton swab to collect secretions from the pharynx or cloacal cavity, put the swab into a centrifuge tube filled with 1.0ml PBS, and send it for inspection immediately. Sec...
Embodiment 2
[0093] Embodiment 2 Sensitivity experiment
[0094] figure 1 It is a sensitivity experiment for the detection of avian influenza virus H7 gene in a four-channel fluorescent PCR system, from left to right is 1×10 6 , 1×10 5 , 1×10 4 , 1×10 3 , 1×10 2 , 1×10 1 Amplification results of standards in cp / μl. It can be seen from the figure that the sensitivity of H7 gene detection is 1×10 2 cp / μl.
[0095] figure 2 It is a sensitivity experiment for the detection of avian influenza virus N9 gene in a four-channel fluorescent PCR system, from left to right is 1×10 6 , 1×10 5 , 1×10 4 , 1×10 3 , 1×10 2 , 1×10 1 Amplification results of standards in cp / μl. It can be seen from the figure that the sensitivity of N9 gene detection is 1×10 2 cp / μl.
[0096] image 3 It is a sensitivity experiment for the detection of avian influenza virus H9 gene in a four-channel fluorescent PCR system, from left to right is 1×10 6 , 1×10 5 , 1×10 4 , 1×10 3 , 1×10 2 , 1×10 1Amplif...
Embodiment 3
[0098] Embodiment 3 specificity experiment
[0099] Figure 5 It is the specific experimental result of the detection of avian influenza virus H7 gene in the four-channel fluorescent PCR system. The detection of H7 antigen, H7N9 cotton swab specimens, and H7N7 cotton swab samples of Harmony Research Institute was positive, and the detection of Harmony Research H5N1 antigen, H5N1 vaccine, H9N2 cotton swab samples, Guangzhou Yongshun NDV vaccine and negative quality control products were all negative.
[0100] Image 6 It is the specific experimental result of the detection of avian influenza virus N9 gene in the four-channel fluorescent PCR system. The detection of H7N9 cotton swab specimens is positive, and the detection of H7N7 cotton swab specimens, Harmony Research H5N1 antigen, Huanong H5N1 vaccine, and H9N2 cotton swab specimens , Guangzhou Yongshun NDV vaccine and negative quality control products were all negative.
[0101] Figure 7 It is the specific experimental ...
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