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Dimethylanthracene-containing organic compound and application thereof

An organic compound, dimethyl anthracene technology, applied in the field of organic optoelectronic materials, can solve different problems such as avoiding aggregation, improving current efficiency and lifespan, improving exciton utilization rate and high fluorescence radiation efficiency

Active Publication Date: 2017-03-01
JIANGSU SUNERA TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition, for the collocation of OLED devices with different structures, the photoelectric functional materials used have strong selectivity, and the performance of the same material in devices with different structures may be completely different.

Method used

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  • Dimethylanthracene-containing organic compound and application thereof
  • Dimethylanthracene-containing organic compound and application thereof
  • Dimethylanthracene-containing organic compound and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0057] Embodiment 1: the synthesis of intermediate A1:

[0058] synthetic route:

[0059]

[0060]

[0061] Add 11.8g of 1,4-dibromobenzene (0.05mol) and 1.33g of Mg powder (0.055mol) and 60ml of tetrahydrofuran to a 250ml four-necked flask under nitrogen atmosphere, heat and reflux for 4 hours, the reaction is complete, and the format Reagent;

[0062] Dissolve 11.1g of 10,10-dimethylanthrone (0.05mol) in 50ml of tetrahydrofuran, add the above-mentioned Grignard reagent dropwise, react at 60°C for 24 hours, a large amount of white precipitate is formed, and finally add saturated NHCl 4 Convert Grignard salt into alcohol; after the reaction, extract with ether, dry and rotary evaporate, petroleum ether: dichloromethane mixed solvent (3:2) silica gel column purification to obtain a slightly yellow solid tertiary alcohol (yield 88%) ; using DEI-MS to identify the compound, formula C 22 h 19 BrO, detection value [M+1] + = 379.03, calculated value 378.06;

[0063] Take...

Embodiment 2

[0064] Embodiment 2: the synthesis of intermediate A2:

[0065] synthetic route:

[0066]

[0067] Intermediate A2 was prepared according to the synthetic method of intermediate A1 in Example 1, the difference being that the compound bromobenzene was replaced by 1,1'-biphenyl;

[0068] Using DEI-MS to identify the compound, formula C 34 h 27 Br, detection value [M+1] + =514.85, calculated value 514.13.

Embodiment 3

[0069] Embodiment 3: the synthesis of intermediate A3:

[0070] synthetic route:

[0071]

[0072] Prepare intermediate A3 by the synthetic method of intermediate A1 among the embodiment 1, difference is to replace bromobenzene with benzene in the third step reaction;

[0073] Using DEI-MS to identify the compound, formula C 28 h 23 Br, detection value [M+1] + =438.10, calculated value 438.87.

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Abstract

The invention discloses a dimethylanthracene-containing compound and an application of the dimethylanthracene-containing compound on an organic electroluminescent device. A structural general formula of the organic compound is shown as a general formula (1). The compound has high glass transition temperature and molecular thermal stability, and appropriate HOMO and LUMO energy level and high Eg, by optimizing a device structure, the photoelectric property of the OLED device and the life of the OLED device are effectively increased.

Description

technical field [0001] The invention relates to the technical field of organic photoelectric materials, in particular to a compound material containing a dimethyl anthracene structure as a central skeleton and its application in the field of OLEDs. Background technique [0002] Organic electroluminescent (OLED: Organic Light Emission Diodes) device technology can be used to manufacture new display products and also can be used to make new lighting products, which is expected to replace the existing liquid crystal display and fluorescent lighting, and has a wide application prospect. [0003] The OLED light-emitting device is like a sandwich structure, including electrode material film layers, and organic functional materials sandwiched between different electrode film layers. Various functional materials are superimposed on each other according to the application to form an OLED light-emitting device. As a current device, when a voltage is applied to the electrodes at both e...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07D209/80C07D209/86C07D491/048C07D487/04C07D495/04C07D517/04C07D519/00C07D491/153C07D495/14C07D487/14C07D513/04C07D498/04C07D471/04C07D491/052C07D491/147C07D491/056C07D491/044C07D471/14C07D498/14C07D513/14C09K11/06H01L51/54
CPCC09K11/06C07D209/80C07D209/86C07D471/04C07D471/14C07D487/04C07D487/14C07D491/044C07D491/048C07D491/052C07D491/056C07D491/147C07D491/153C07D495/04C07D495/14C07D498/04C07D498/14C07D513/04C07D513/14C07D517/04C07D519/00C09K2211/104C09K2211/1037C09K2211/1044C09K2211/1033C09K2211/1029C09K2211/1011C09K2211/1007H10K85/657H10K85/6572
Inventor 张兆超李崇叶中华张小庆王立春
Owner JIANGSU SUNERA TECH CO LTD
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