Indole quinoxaline oganic light emitting diode material
A technology of light-emitting diodes and light-emitting materials, which is applied in the direction of organic light-emitting devices, organic light-emitting device structures, materials for organic semiconductor devices, etc., and can solve problems such as difficult film formation and poor solubility
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Embodiment 1
[0087] Example 1: Synthetic preparation of compounds.
[0088] According to chemical reaction formulas 6 and 7, intermediate compounds A6-1 and B6-1 were prepared respectively, and finally compound 2-1 was prepared in reaction formula 8 with 82% yield.
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[0092] Similarly, based on the above principles of synthetic chemistry, without departing from the scope of the present invention, the following main material compounds were synthesized. The specific listed compounds have molecular weights and molecular fragments verified by mass spectrometry, as shown in Table 3 below.
[0093] Table 3: Compound synthesis and characterization:
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Embodiment 2
[0105] Embodiment 2 Device application example.
[0106] In a background vacuum up to 10 -5 Pa's multi-source evaporation OLED preparation equipment adopts the following device structure: ITO / mTDATA (100 Å) / NPD (400 Å) / Host: 5% luminescent dopant 10% (300 Å ) / TPBi (300 Å) / LiF (10Å) / Al, using different Host OLED light-emitting devices for comparison. Wherein the vacuum deposition speed of each organic layer and electrode is listed in Table 4 at time.
[0107] Compare the main material:
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[0109] Table 4: Preparation conditions of OLED devices (doping wt concentration in the light-emitting layer is 9%).
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[0111] For cross-linkable host materials, use host material and luminescent dopant solution, such as 15% (weight) xylene solution, use spin coating and then heat in a nitrogen glove box to evaporate the solvent and complete cross-linking into an insoluble and infusible luminescent layer film.
[0112] All manufactured OLED devices are tested and ...
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