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Finishing method of flame-retardant real silk fabric and application of finishing

A technology of silk fabrics and flame retardancy, which is applied in the field of finishing of flame-retardant silk fabrics, can solve the problems that cannot meet the requirements of flame-retardant textiles, and achieve good flame-retardant effects

Active Publication Date: 2017-05-31
江苏华佳控股集团有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, they still belong to the category of flammable textiles and cannot meet people's demand for flame-retardant textiles. Therefore, it is necessary to perform flame-retardant finishing on real silk fabrics.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Finishing method of flame-retardant real silk fabric and application of finishing
  • Finishing method of flame-retardant real silk fabric and application of finishing
  • Finishing method of flame-retardant real silk fabric and application of finishing

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Dissolve 4.5g of boron phosphate in 50mL of deionized water at 80°C, stir continuously until the solution is colorless, then add the dissolved mixed solution dropwise to 100mL of industrial silica sol, and react at 80°C for 3h , and finally the fabric is immersed in the prepared doped silica sol for 10 minutes, and is finished by the finishing process of two dipping and two rolling (residue rate 90% to 100%)→pre-baking at 80°C for 3 minutes→baking at 180°C for 3 minutes.

[0028] The fabric used in the present invention is real silk 10m / m electric spinning.

[0029] After testing, the limiting oxygen index of the finished silk fabric is 32.4%, and after 30 times of washing, the limiting oxygen index is 24.2%. in addition. In the fabric vertical burning test, the damaged length of the unfinished silk fabric is 30 cm, and the damaged length of the finished silk fabric is 11.7 cm.

Embodiment 2

[0031] Dissolve 4.5g of boron phosphate, 7.5g of citric acid monohydrate, 6g of tartaric acid, and 6.75g of sodium hypophosphite in 50mL of deionized water at 80°C until the solution is colorless, then add the dissolved mixed solution dropwise to 100mL of industrial Use silica sol, and react at 80°C for 3 hours, and finally immerse the fabric in the prepared doped silica sol for 10 minutes, and use two dipping and two padding (reduction rate 90% to 100%) → 80°C pre-baking 3min → 180°C baking 3min finishing process for finishing.

[0032] The fabric used in the present invention is real silk 10m / m electric spinning.

[0033] After testing, the limiting oxygen index of the finished silk fabric is 31.1%, and after 30 times of washing, the limiting oxygen index is 26.6%. in addition. In the fabric vertical burning test, the damaged length of the unfinished silk fabric is 30 cm, and the damaged length of the finished silk fabric is 12.9 cm.

Embodiment 3

[0035] Dissolve 4.5g of boron phosphate, 7.5g of citric acid monohydrate, 3g of tartaric acid, and 6.75g of sodium hypophosphite in 50mL of deionized water at 80°C until the solution is colorless, then add the dissolved mixed solution dropwise to 100mL of industrial Use silica sol, and react at 80°C for 3 hours, and finally immerse the fabric in the prepared doped silica sol for 10 minutes, and use two dipping and two padding (reduction rate 90% to 100%) → 80°C pre-baking 3min → 180°C baking 3min finishing process for finishing.

[0036] The fabric used in the present invention is real silk 10m / m electric spinning.

[0037] After testing, the limiting oxygen index of the finished silk fabric is 28.9%. After 30 times of washing, the limiting oxygen index is 25.8%. In the fabric vertical burning test, the damaged length of the finished silk fabric is 14.3cm.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention discloses a finishing method of flame-retardant real silk fabric and an application of the finishing. The method comprises the processes of preparing a finishing liquid, preparing the finishing liquid / silica sol, and finishing the real silk fabric, and application of the method in improving the fire resistance of the real silk fabric. The real silk fabric prepared by the finishing method has certain durability. Reagents adopted by the finishing method all are nontoxic and harmless green products, so that green and environment-friendly preparation processes are ensured. The finishing method is suitable for industrial finishing of the real silk fabric.

Description

technical field [0001] The invention belongs to the technical field of textile chemistry and relates to a new fabric finishing method, in particular to a finishing method of flame-retardant silk fabric and its application. Background technique [0002] The rapid economic development is accompanied by prominent environmental problems. In the 21st century, people pay more and more attention to the environment. Therefore, the textiles that are closely related to everyone's life are the first thing people pay attention to. The environmental problems and hazards caused by fabric burning have also been paid more attention to. These demands have prompted printing and dyeing textile workers to develop flame-retardant textiles with higher standards, more effective, durable and without affecting the feel and comfort of fabrics, which is of great significance to human beings and the living environment. [0003] Real silk is a natural fiber with excellent performance. Compared with cel...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M11/80D06M13/207D06M11/79D06M101/10
CPCD06M11/79D06M11/80D06M13/207D06M2101/10D06M2200/30
Inventor 邢铁玲俞金键陈云博陈国强谈金麒
Owner 江苏华佳控股集团有限公司
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