Method for recovering silicon carbide
A recycling method and silicon carbide technology, applied in the field of recycling, can solve problems such as toxicity and low flash point, and achieve the effects of reducing material waste, material loss, energy consumption and recycling cost.
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Embodiment 1
[0049] One of the silicon carbide recovery methods of the present invention, the silicon carbide recovery method comprises a filtration step S1, a raffinate removal step S2, and a pickling and impurity removal step
[0050] S3, silicon dissolving step S4 and lye removing step S5.
[0051] 1. Filtration step S1
[0052] (1) Filtrating the silicon-containing mortar containing silicon carbide, silicon, impurities and dispersion to obtain a silicon carbide / silicon mixture from which the dispersion is initially filtered;
[0053]In more detail, the silicon-containing mortar is the cutting waste liquid for cutting silicon crystal rods, so the silicon-containing mortar contains silicon carbide, silicon and a dispersion liquid. The dispersion liquid is a commonly used cutting liquid, such as polyethylene glycol ( PEG) and other cutting fluids, silicon-containing mortar may also contain other impurities, such as debris generated by cutting tools, usually iron filings or other metal de...
Embodiment 2
[0068] The recovery method two of silicon carbide of the present invention
[0069] The second method of recovering silicon carbide of the present invention comprises a filtering step S1, a raffinate removal step S2, an pickling and impurity removal step S3, a stirring step S21, a silicon dissolving step S4, and a lye removal step S5.
[0070] 1. The filtering step S1 is the same as the filtering step S1 described in Example 1.
[0071] 2. The residual liquid removal step S2 is the same as the residual liquid removal step S2 described in Example 1.
[0072] 3. The pickling and impurity removal step S3 is the same as the pickling and impurity removal step S3 described in Example 1.
[0073] 4. Stirring step S21
[0074] Add the impurity-removed silicon carbide / silicon mixture into an aqueous medium with a pH of 2.5 to 14, stir evenly, and then let it stand to obtain a precipitated silicon carbide / silicon mixture and a liquid medium in which silicon is suspended. Filter the pr...
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